Last Step towards Macrocyclic Glycoterpenoids Having Isosteviol and Glucosamine Moieties

Garifullin, B. F.; Strobykina, I. Yu.; Sharipova, R. R.; Bazanova, Olga B.; Катаев, В. Е.

doi:10.6060/mhc151198k

Cited by 2 publications

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“…The residue was diluted with CH 2 Cl 2 , washed with 5 % NaHCO 3 and water and brine, dried over Na 2 SO 4 ). ‡ Macrocyclic glycoterpenoid (5) ), 5.82 (d, 2H, J = 9.3 Hz, 2NH). NMR experiments were carried out with Avance-400 and Avance-500 (Bruker) spectrometers.…”

Section: Notes and References †mentioning

confidence: 99%

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The First Macrocyclic Glycoterpenoid Having Glucosamine and Isosteviol Moieties

Garifullin¹,

Strobykina²,

Sharipova³

et al. 2016

MHC

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Section: Notes and References †mentioning

confidence: 99%

“…[5] For the macrocyclization of diglycoside 3 its protecting groups were removed by the reaction with activated powdered zinc in glacial acetic acid, and diglycoside 4 were obtained in 87 % yield. † 2 atoms of glucosamine residues were shifted upfield in keeping with the literature data, [6,7] and resonated as a doublet of doublets at 2.…”

mentioning

confidence: 99%

The First Macrocyclic Glycoterpenoid Having Glucosamine and Isosteviol Moieties

Garifullin¹,

Strobykina²,

Sharipova³

et al. 2016

MHC

Self Cite

View full text Add to dashboard Cite

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Analysis of Carbohydrates and Glycoconjugates by Matrix‐assisted Laser Desorption/Ionization Mass Spectrometry: An Update for 2015–2016

Harvey

2021

Mass Spectrometry Reviews

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This review is the ninth update of the original article published in 1999 on the application of matrix‐assisted laser desorption/ionization (MALDI) mass spectrometry to the analysis of carbohydrates and glycoconjugates and brings coverage of the literature to the end of 2016. Also included are papers that describe methods appropriate to analysis by MALDI, such as sample preparation techniques, even though the ionization method is not MALDI. Topics covered in the first part of the review include general aspects such as theory of the MALDI process, matrices, derivatization, MALDI imaging, fragmentation and arrays. The second part of the review is devoted to applications to various structural types such as oligo‐ and poly‐saccharides, glycoproteins, glycolipids, glycosides and biopharmaceuticals. Much of this material is presented in tabular form. The third part of the review covers medical and industrial applications of the technique, studies of enzyme reactions and applications to chemical synthesis. The reported work shows increasing use of combined new techniques such as ion mobility and the enormous impact that MALDI imaging is having. MALDI, although invented over 30 years ago is still an ideal technique for carbohydrate analysis and advancements in the technique and range of applications show no sign of deminishing. © 2020 Wiley Periodicals, Inc.

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Last Step towards Macrocyclic Glycoterpenoids Having Isosteviol and Glucosamine Moieties

Abstract: The first diglycosides possessing two glucosamine residues and two moieties of diterpenoid isosteviol have beenКлючевые слова: Терпеноиды, изостевиол, глюкозамин, гликоконъюгаты, гликотерпеноиды.

Cited by 2 publications

References 19 publications

The First Macrocyclic Glycoterpenoid Having Glucosamine and Isosteviol Moieties

The First Macrocyclic Glycoterpenoid Having Glucosamine and Isosteviol Moieties

Analysis of Carbohydrates and Glycoconjugates by Matrix‐assisted Laser Desorption/Ionization Mass Spectrometry: An Update for 2015–2016

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