2010
DOI: 10.1039/c002054k
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Lanthanide–organic assemblies with pyrazinetetracarboxylic and benzophenone-3,3′,4,4′-tetracarboxylic acids

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Cited by 17 publications
(10 citation statements)
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“…As reported in the literature, 37 the powder of Eu-HBPTC was prepared as follows: 32 mg (0.1 mmol) benzophenone-3,3 0 ,4,4 0tetracarboxylic dianhydride (BTDA), 45 mg (0.1 mmol) europium nitrate hexahydrate and demineralized 2 mL water were placed in a 10 mL Teon-lined stainless-steel vessel and heated at 180 C for 3 days under autogenous pressure. Aer the reaction mixture was cooled down to room temperature, the powder of Eu-HBPTC was ltered off, washed with distilled water, and dried in air.…”
Section: Synthesis Of Eu-hbptc Powdermentioning
confidence: 99%
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“…As reported in the literature, 37 the powder of Eu-HBPTC was prepared as follows: 32 mg (0.1 mmol) benzophenone-3,3 0 ,4,4 0tetracarboxylic dianhydride (BTDA), 45 mg (0.1 mmol) europium nitrate hexahydrate and demineralized 2 mL water were placed in a 10 mL Teon-lined stainless-steel vessel and heated at 180 C for 3 days under autogenous pressure. Aer the reaction mixture was cooled down to room temperature, the powder of Eu-HBPTC was ltered off, washed with distilled water, and dried in air.…”
Section: Synthesis Of Eu-hbptc Powdermentioning
confidence: 99%
“…However, the XRD patterns show poor crystallinity but generally matches the theoretical spectrum. 37,45 The lack of crystallinity could be due to the lm drying before or during XRD analysis, leading to lm degradation. 23 Attempts to improve crystallinity of Eu-HBPTC lms and powder have thus far been unsuccessful.…”
Section: Powder X-ray Diffraction and Ft-ir Analysesmentioning
confidence: 99%
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“…24,[28][29][30][31][32][33] Also, in our attempts to synthesize structures that incorporate 3,6-dimethylpyrazine-2,5-dicarboxylate and/or 2,2′-bpyridine as co-ligands in similar mole ratios as above, it was observed that the structures were resistant to incorporating these additional ligands under the synthesis conditions explored, as indicated by single crystal X-Ray analysis. In addition to the ligand to metal mole ratio of 1 : 0.75 used for the structures of 1 and 2, syntheses were also conducted using ratios of 1 : 1.3, 1 : 1.5 and 1 : 2.0.…”
Section: Synthesismentioning
confidence: 99%
“…The fully deprotonated ligand is widely reported for the synthesis of CPs and MOFs mainly in combination with selected s-and d-block metal ions. 30 They also reported the use of the actinide element, uranium, (as UO 2 species) in the synthesis of a 3-D IJUO 2 ) 2 -pztc MOF structure. 27 All, except Cd, crystallize as 1-D chains or 2-D layered CPs.…”
Section: Introductionmentioning
confidence: 99%