Laboratory spray drying of materials for batteries, lasers, and bioceramics

Arpagaus, Cordin; Collenberg, Andreas; Rütti, David

doi:10.1080/07373937.2017.1410487

Cited by 8 publications

(4 citation statements)

References 30 publications

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“…Both scientific approaches [5,7,8] and industrial applications [9] are covered to meet the needs of industry as well as academia. As expected, there has been emphasis on various aspects of freeze drying [10,11] and spray drying [12] in the food and pharmaceutical sectors.…”

Section: Role Of Critical Reviews In Encouraging Appropriate Randdmentioning

confidence: 74%

Role of critical reviews in encouraging appropriate R&D

2019

Drying Technology

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Section: Role Of Critical Reviews In Encouraging Appropriate Randdmentioning

confidence: 74%

Role of critical reviews in encouraging appropriate R&D

2019

Drying Technology

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“…In the primary scientific literature, the most common systems are home-made equipment, commercial table-top systems [368,369] and commercial (small) pilot-scale systems. As an example, our group started working on spray-drying at the beginning of the 2000s with a table-top Buchi Mini Spray-dryer B-190 (Büchi Labortechnik AG, Switzerland) and now owns two Mobile Minor TM units, which can evaporate up to 5.5 kg H 2 O per hour and correspond to the smallest-but-one R&D systems on the catalogue of a provider of industrial spray-drying technology (GEA).…”

Section: Experimental Parameters In Spray-dryingmentioning

confidence: 99%

“…should also be reported. A recent review by Arpagaus et al [368] includes a section about electrode materials, focusing on a few publications where detailed spray-drying parameters are provided together with data on particle morphology and electrochemical performance. In most papers, however, information on the spray-drying parameters is missing or incomplete as illustrated by Table A1 in Appendix A for the case of layered oxide compounds.…”

Section: Experimental Parameters In Spray-dryingmentioning

confidence: 99%

Spray-Drying of Electrode Materials for Lithium- and Sodium-Ion Batteries

et al. 2018

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The performance of electrode materials in lithium-ion (Li-ion), sodium-ion (Na-ion) and related batteries depends not only on their chemical composition but also on their microstructure. The choice of a synthesis method is therefore of paramount importance. Amongst the wide variety of synthesis or shaping routes reported for an ever-increasing panel of compositions, spray-drying stands out as a versatile tool offering demonstrated potential for up-scaling to industrial quantities. In this review, we provide an overview of the rapidly increasing literature including both spray-drying of solutions and spray-drying of suspensions. We focus, in particular, on the chemical aspects of the formulation of the solution/suspension to be spray-dried. We also consider the post-processing of the spray-dried precursors and the resulting morphologies of granules. The review references more than 300 publications in tables where entries are listed based on final compound composition, starting materials, sources of carbon etc.

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“…Raw materials for ceramic tiles, clays for whitewares, detergents, and milk powder are examples of high-volume products which are manufactured on a large scale using the spray drying process. Recently, spray drying has been successfully utilized for the production of high-value particles including layered double hydroxide adsorbents [21], hydroxyapatite agglomerates for scaffold manufacturing [20,28], alumina/zirconia ceramic composites for orthopedic applications [8,9], and electrode materials for lithium-ion batteries [3]. The spray drying is the energy-intensive process because a large amount of energy is consumed for water evaporation.…”

Section: Introductionmentioning

confidence: 99%

An Excel VBA‐based educational module for simulation and energy optimization of spray drying process

Golman

Yermukhambetova

2019

Comp Applic In Engineering

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The spray drying processes are widely used in chemical, ceramic, food, and pharmaceutical industries to produce both high-volume and high-value particulate products. Therefore, it is important to include a topic covering the spray drying process in the undergraduate curriculum of chemical and materials engineering students. In this article, we describe an Excel Visual Basic for Applications (VBA)-based educational module developed to assist students in learning the spray drying process. The module consists of two Excel files with VBA macro programs and teaching materials. The module focuses on the design of spray drying process conditions to produce the particulate product with desired moisture content at required production rate while satisfying the process restrictions on the inlet slurry concentration and the exhaust air temperature. Students are also asked to carry out the energy performance analysis of spray dryer equipped with an air-to-air heat exchanger that recovers the exhaust air heat to preheat the drying air. Using this module, students will enhance their theoretical and practical knowledge in drying processes, and gain analytical skills in drying process energy optimization. K E Y W O R D Senergy recovery, Excel VBA simulator, mass and energy balances, modeling, spray drying

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Laboratory spray drying of materials for batteries, lasers, and bioceramics

Cited by 8 publications

References 30 publications

Role of critical reviews in encouraging appropriate R&D

Role of critical reviews in encouraging appropriate R&D

Spray-Drying of Electrode Materials for Lithium- and Sodium-Ion Batteries

An Excel VBA‐based educational module for simulation and energy optimization of spray drying process

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