Abstract:Kinetics and mechanism of gold electrooxidation in sulfuric acid solutions of thiocarbamide ( TCA ) are studied by measuring voltammograms ( VA ) of gold and glassy carbon ( GC ) electrodes. In a potential ( E ) range from -0.2 to 1.2 V ( SCE ), VA of a gold electrode demonstrate three peaks. The first and the second peaks correspond to gold electrooxidation to [AuTCA ads ] + and [Au(TCA ads ) 3 ] 3+ ions at E of 0.152 and 0.554 V, while the third one corresponds to TCA electrooxidation. The electrooxidation o… Show more
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