IR Study of Complex Between Salicylalbenzoylhydrazone (SBH) and Iron III: Normal Mode Assignment Assisted by Quantum Mechanical Calculation

Vauthier, E.; Maurel, François; Couesnon, Thierry; Cossé-Barbi, Aliette

doi:10.1080/00387019909350002

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“…= 0.04, n = 70). Elemental analysis 19 and infrared spectroscopy 20 further confirmed this stoichiometry.…”

Section: ■ Hazardsmentioning

confidence: 55%

Synthesis and Characterization of Metal Complexes with Schiff Base Ligands

2015

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In order for undergraduate laboratory experiments to reflect modern research practice, it is essential that they include a range of elements, and that synthetic tasks are accompanied by characterization and analysis. This intermediate general chemistry laboratory exercise runs over 2 weeks, and involves the preparation of a Schiff base ligand and its metal (Fe 3+ or Cu 2+ ) complex. Students are then able to determine the metal−ligand stoichiometry of one metal− ligand pair. This experiment demonstrates that varying the transition metal can give rise to different structures, and hence different properties.

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“…= 0.04, n = 70). Elemental analysis 19 and infrared spectroscopy 20 further confirmed this stoichiometry.…”

Section: ■ Hazardsmentioning

confidence: 55%