Abstract:In the present work, electrocatalytic properties of Pt-EG and Pt/Mo-EG composite electrodes are studied. These composites were prepared by a three-step synthesis. First, stage-1 HClO4-GIC was synthesized using the chronopotentiometric method. Then, HClO4-GIC was heat treated to obtain expanded graphite. Finally, expanded graphite was coated with platinum catalyst from a water-alcohol solution of H2PtCl6. MoCl5-GIC synthesized in parallel was subjected to thermal exfoliation to get Mo-EG composite onto which pl… Show more
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