Intensification of fructose dehydration into 5‐HMF and subsequent oxidation to 2,5‐FDCA using ultrasound
Danwyn J. Aranha,
Madhuri M. Kininge,
Parag R. Gogate
Abstract:Ultrasound‐assisted dehydration of fructose into 5‐hydroxymethylfurfural (5‐HMF) and subsequent oxidation to furandicarboxylic acid (2, 5‐FDCA) is studied in the current work with the main objective being to elucidate the effectiveness of ultrasound for intensified synthesis. The effect of reaction parameters like ultrasound power, duty cycle, reaction time, reaction temperature, solid to solvent ratio, and fructose concentration on the dehydration of fructose into 5‐HMF has been studied. Optimized conditions … Show more
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