Inorganofunctionalization of Ti(IV) and Zr(IV) on the MCM-41 Surface and its Interaction with a Mixed Valence Complex to use as Isoniazid Sensing

Magossi, Maiara de Souza; Fernandes, Daniela Silvestrini; Franco, Fernanda dos Santos; Felipe, Alexsandro dos Santos; Vicente, F.; Carmo, Devaney Ribeiro do

doi:10.1007/s10904-021-02025-x

Cited by 2 publications

(3 citation statements)

References 38 publications

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“…), represented by Equations 1 and 2, respectively. The process occurs as described by Magossi et al [25] and Fernandes et al [35].…”

Section: Catalytic Isoniazid Electrooxidationmentioning

confidence: 98%

“…The material surface areas and porosities were assessed according to Magossi et al [25] employing a Micromeritics ASAP 2010 pore analyzer.…”

Section: Porosity and Surface Areamentioning

confidence: 99%

“…In the treatment of tuberculosis, isoniazid (pyridine-4-carboxylic acid hydrazide) is one of the most effective agents. It is usually prescribed in order to prevent the development of clinical tuberculosis [25]. The action of isoniazid may be either bacteriostatic or bacteriocidal, depending on the concentration of the drug attained at the site of infection and the susceptibility of the infecting organism to the drug.…”

Section: Introductionmentioning

confidence: 99%

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Behaviour of the faujasite zeolite occluded with Ti(IV) and Zr(IV) and its interaction with Nickel Hexacyanoferrate (III) : A comparative study in the voltammetric detection of isoniazid

Magossi

Vicente

Carmo

2023

Preprint

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This study describes titanium and zirconium incorporations into a FAU zeolite and subsequent modification with nickel hexacyanoferrate.The obtained materials (ZTiNiH and ZZrNiH) were characterized by Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM), X-ray Dispersive Energy Spectroscopy (EDS), Porosity and Surface Area and Cyclic Voltammetry (CV). The cyclic voltammograms applied to the modifed ZTiNiH and ZZrNiH graphite pastes indicate sensitivity to isoniazid (IZN). The modifed ZTiNiH graphite paste electrode displayed a linear analytical curve response from 4.0× 10–5 to 7.0× 10–4 mol L− 1 and limit of detection of 4.9×10− 5 mol L− 1, while the modified ZZrNiH electrode presented a linear analytical curve response from 1.0×10− 5 a 3.0×10− 4 mol L− 1 and limit of detection of 2.0×10− 5 mol L− 1. After catalytic IZN electro-oxidation, a study concerning the main IZN interferents was performed and its recovery from a synthetic urine sample was assessed. The obtained ZTiNiH and ZZrNiH materials are noteworthy for their good limit of detection and recovery eficiency when applied to real samples, thus comprising potential candidates for the development of electrochemical sensors aiming at IZN detection.

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“…), represented by Equations 1 and 2, respectively. The process occurs as described by Magossi et al [25] and Fernandes et al [35].…”

Section: Catalytic Isoniazid Electrooxidationmentioning

confidence: 98%

“…The material surface areas and porosities were assessed according to Magossi et al [25] employing a Micromeritics ASAP 2010 pore analyzer.…”

Section: Porosity and Surface Areamentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

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Behaviour of the faujasite zeolite occluded with Ti(IV) and Zr(IV) and its interaction with Nickel Hexacyanoferrate (III) : A comparative study in the voltammetric detection of isoniazid

Magossi

Vicente

Carmo

2023

Preprint

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New method of identifying morphine in urine samples using nanoparticle-dendrimer-enzyme hybrid system

Tahmasebi

Esmaeili

Bambai

2022

Arabian Journal of Chemistry

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Inorganofunctionalization of Ti(IV) and Zr(IV) on the MCM-41 Surface and its Interaction with a Mixed Valence Complex to use as Isoniazid Sensing

Cited by 2 publications

References 38 publications

Behaviour of the faujasite zeolite occluded with Ti(IV) and Zr(IV) and its interaction with Nickel Hexacyanoferrate (III) : A comparative study in the voltammetric detection of isoniazid

Behaviour of the faujasite zeolite occluded with Ti(IV) and Zr(IV) and its interaction with Nickel Hexacyanoferrate (III) : A comparative study in the voltammetric detection of isoniazid

New method of identifying morphine in urine samples using nanoparticle-dendrimer-enzyme hybrid system

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