2016
DOI: 10.1515/rrlm-2016-0041 View full text |Buy / Rent full text
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Abstract: Cassia mimosoides Linn has been used from ancient times and used for treating hepatitis for its supposedly medically beneficial properties. In this study, different constituents of the Cassia mimosoides Linn (β-Sitosterol, Oleanolic Acid, Emodin, Carotene, Resorcinol, Luteolin, and α-L-Rhamnose)

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“…Our sequential chromatographic experiments on the active fractions led to the isolation of 10 compounds, one of which was a mixture (Figure 1). Our structure elucidation studies indicated that five of them were abietane-type diterpenes (6,7-dehydroyleanone (1) [23], ferruginol (3) [24], horminone-7-acetoxyhorminone mixture (1:1) (6) (which were previously isolated from several Salvia species), 7-acetoxyhorminone (7) [25][26][27], and pisiferal (8) [28]); two nor abietane-type diterpenes (12-demethylmulticaulin (2) [29,30], and 12-hydroxy abieta-1, 3, 5 (10) 8, 11, 13-hexaene (4) [30,31]); one steroid (β-sitosterol (5) [32]); and two triterpenes (ursolic acid (9) [32] and oleanolic acid (10) [32]). Their structures were revealed using a combination of spectroscopic methods, e.g., UV, IR, 1 H-and 13 C-NMR-APT, HMQC, HMBC, and mass spectrometry (MS).…”
Section: Structure Elucidationmentioning
“…β-Sitosterol, as a white powder (8 mg) (5), and a mixture of horminone and 7-acetoxyhorminone (1:1) (15 mg, orange crystal) (6), were isolated from the M-6 fraction (petroleum ether-dichloromethane: 1/2 solvent system) with the help of preparative thin layer chromatography (TLC). 7-Acetoxyhorminone (7) was isolated from the M-7 fraction as an orange crystal (10 mg) using a Sephadex column, followed by preparative TLC (petroleum ether-dichloromethane: 1/3). Pisiferal (8) was isolated from the M-8…”
Section: Isolation Of the Compoundsmentioning
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