Influences of CO2 Bubbling Types on Preparation of Calcite Nanoparticles by Carbonation Process

Altıner, Mahmut

doi:10.3311/ppch.10664

Cited by 16 publications

(12 citation statements)

References 29 publications

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“…The carbonation process is ended if the pH of the solution has not changed. Carbonation reaction following previous research [15,16].…”

Section: Resultsmentioning

confidence: 99%

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Synthesis and Characterization of Precipitated CaCO3 from Ankerite Prepared by Bubbling Method

Munawaroh¹,

Muharrami²,

Triwikantoro³

et al. 2019

KEG

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“…The carbonation process is ended if the pH of the solution has not changed. Carbonation reaction following previous research [15,16].…”

Section: Resultsmentioning

confidence: 99%

“…One way for the synthesis of PCC is bubbling method. Many researchers have used it [15][16][17][18]. The bubbling method is to flow CO 2 gas into spherical bubbles to the solution.…”

Section: Introductionmentioning

confidence: 99%

Synthesis and Characterization of Precipitated CaCO3 from Ankerite Prepared by Bubbling Method

Munawaroh¹,

Muharrami²,

Triwikantoro³

et al. 2019

KEG

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“…It shows faster precipitation of calcite and produces smaller particles than the ordinary carbonation method. 14 Large bubbles have buoyant behavior in solution, making them difficult to dissolve and easily broken, whereas tiny bubbles can maintain their presence in solution, making them easier to dissolve. 15 Synthesis of calcite via fine bubble carbonation has been applied.…”

Section: Introductionmentioning

confidence: 99%

Preparation of micro-calcite powder using fine-bubble assisted carbonation as toothpaste material

et al. 2023

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Introduction: Calcite (CaCO3) is typically used in commercial toothpaste with particle size ranges from 1-12 μm. In the latest study, calcite was synthesized by using Ca(OH)2 precursor from natural resources However, the resulting particle size does not match the size of the toothpaste filler. This study aims to prepare micro-calcite from Ca(OH)2 analytical grade precursor via fine-bubble assisted carbonation and analysis the effect of precursor concentration and pH on the particle size of the calcite Methods: The calcite powder was prepared from Ca(OH)2 analytical grade powder utilizing the fine-bubble carbonation process with the Ca(OH)2 concentration and initial pH variation. The study was started by making a Ca(OH)2 suspension with a concentration of 0.25, 0.5, 0.75, 1 and 1.25 M using 2.000 ml methanol as a solvent. 0.5 M NaH2PO4 solutions were utilized to adjust the initial pH of 0.5 M Ca(OH)2 suspension into 8, 9, and 10. The suspensions were aerated using CO2 fine-bubble for two hours to produce CaCO3 samples. All precipitated CaCO3 particles were characterized by PSA, Zeta-Potential, and FTIR measurements Results: The calcite phase was identified from the FTIR transmittance. Aragonite or vaterite phase was not observed in the samples. PSA result shows the size of CaCO3 particles from samples 0.25 M to 1.25 M are as follows 3.03, 3.23, 2.79, 3.70, 0.99 μm respectively. Meanwhile, the particle sizes of CaCO3 in samples with a pH of 8, 9 and 10 are 3.00, 2.03 and 2.50 μm respectively. The zeta potential shows the value ranges from -23.2 mV to -11.9 mV, indicating fair dispersion ability. Conclusion: The fine bubble assisted carbonation method in this study helps in producing calcite particle sizes that could be used as alternative fillers for toothpaste.Keywords: calcite, fine-bubble, carbonation, particle size, toothpaste

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“…Another approach to CaCO 3 synthesis is the carbonation method, i.e., the absorption of CO 2 microbubbles into Ca(OH) 2 solution. 49 Microbubbles are spherical bubbles smaller than 100 mm in diameter that can be uniformly distributed in a liquid. 50 A microbubble generator produces innumerable micro-size bubbles, and the solubility of CO 2 is increased.…”

Section: Introductionmentioning

confidence: 99%

Calcium carbonate particles: synthesis, temperature and time influence on the size, shape, phase, and their impact on cell hydroxyapatite formation

et al. 2021

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Influences of CO2 Bubbling Types on Preparation of Calcite Nanoparticles by Carbonation Process

Abstract: This study investigates the comparison of influences of CO

Cited by 16 publications

References 29 publications

Synthesis and Characterization of Precipitated CaCO3 from Ankerite Prepared by Bubbling Method

Synthesis and Characterization of Precipitated CaCO3 from Ankerite Prepared by Bubbling Method

Preparation of micro-calcite powder using fine-bubble assisted carbonation as toothpaste material

Calcium carbonate particles: synthesis, temperature and time influence on the size, shape, phase, and their impact on cell hydroxyapatite formation

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