Abstract:Dental pieces are subjected to constant friction due to grinding during mastication and mouth disorders such as bruxism. Therefore, wear resistance of Y-TZP materials used for dental prostheses must be investigated. In this work, the influence of humidity and low temperature hydrothermal degradation (LTD) in 3Y-TZP ceramics subjected to fretting has been evaluated. A 100% r.h. reduces the effects of wear due to the lubricative effect of water, compared to those at ambient r.h. COF, wear volume and damage are c… Show more
“…However, an important characteristic of these materials is completely stabilized zirconia tetragonal (t) phase with the addition of an oxide (Y 2 O 3 , CeO 2 ,…), for example, with ~3.0 mol% of yttria for dental applications. This is important because when Y-TZP materials are subjected to humidity at 25-280°C [14][15][16], a sharp decline in their mechanical properties occurs over time. This phenomenon is referred to as low-temperature degradation (LTD) [17,18].…”
Ceramics are increasingly used as structural materials with biomedical applications due to their mechanical properties, biocompatibility, esthetic characteristics and durability. Specifically, zirconia-based compounds are commonly used to develop metal-free restorations and dental implants. The consolidation of ceramics is usually carried out through powders by means of processes that require a lot of energy, as long as processing times and high temperatures (over 1400°C) are required. In the recent years, new research is being developed in this field to reduce both energy consumption and processing time of ceramic powders. One of the most promising techniques for sintering ceramics is microwave heating technology. The main objective of this chapter is to obtain highly densified zirconia-alumina compounds by microwave technology. After sintering, the materials are characterized to determine whether the final properties meet the mechanical requirements for their final applications as dental material. Finally, the characterization of specimens treated by low-temperature degradation (LTD) is carried out after each 20 h of LTD exposure up to 200 h. In addition, the quantification of monoclinic phase by micro-Raman spectroscopy, analysis by AFM and Nomarski optical microscopy and assessment of the roughness and mechanical properties (hardness and Young’s modulus) by nanoindentation technique have been studied.
“…However, an important characteristic of these materials is completely stabilized zirconia tetragonal (t) phase with the addition of an oxide (Y 2 O 3 , CeO 2 ,…), for example, with ~3.0 mol% of yttria for dental applications. This is important because when Y-TZP materials are subjected to humidity at 25-280°C [14][15][16], a sharp decline in their mechanical properties occurs over time. This phenomenon is referred to as low-temperature degradation (LTD) [17,18].…”
Ceramics are increasingly used as structural materials with biomedical applications due to their mechanical properties, biocompatibility, esthetic characteristics and durability. Specifically, zirconia-based compounds are commonly used to develop metal-free restorations and dental implants. The consolidation of ceramics is usually carried out through powders by means of processes that require a lot of energy, as long as processing times and high temperatures (over 1400°C) are required. In the recent years, new research is being developed in this field to reduce both energy consumption and processing time of ceramic powders. One of the most promising techniques for sintering ceramics is microwave heating technology. The main objective of this chapter is to obtain highly densified zirconia-alumina compounds by microwave technology. After sintering, the materials are characterized to determine whether the final properties meet the mechanical requirements for their final applications as dental material. Finally, the characterization of specimens treated by low-temperature degradation (LTD) is carried out after each 20 h of LTD exposure up to 200 h. In addition, the quantification of monoclinic phase by micro-Raman spectroscopy, analysis by AFM and Nomarski optical microscopy and assessment of the roughness and mechanical properties (hardness and Young’s modulus) by nanoindentation technique have been studied.
“…Ding et al [ 22 ] showed that the partial slip region was always associated with slight wear, the mixed region formed cracks, and the gross slip region mainly produced wear and damage of materials. A lot of studies showed that there were many influencing factors on the fretting wear behavior of materials, including frequency [ 23 , 24 ], normal force [ 25 , 26 ], displacement amplitude [ 27 , 28 ], and even temperature [ 29 , 30 ], surface roughness and so on [ 31 , 32 , 33 , 34 , 35 ].…”
This paper discusses an in-depth experimental study on the fretting wear behavior of PVDF (polyvinylidene fluoride) piezoelectric thin film against a Si3N4 ceramic sphere under air conditions. A fretting wear device with a ball-on-plate contact configuration was applied. The changes of displacement amplitude, normal force, and applied voltage were taken into account. The friction logs were used to determine the contact state of the PVDF thin film during the fretting test. The 3D topography instrument and scanning electron microscope (SEM) were used to measure the details of the surface morphology and wear volume. The test results of PVDF thin films under different normal force, displacement amplitude, and applied voltage are summarized through the collection and analysis of experimental data. It is shown that the creep and plastic deformation lead to obvious winkles at the contact surface, which may decrease the specific wear rate of PVDF thin films.
“…Despite zirconia's good mechanical, chemical and esthetic properties, more information is required regarding the effects that LTD might produce, a phenomenon known to cause spontaneous "ageing" and loss of mechanical properties in this material [17]. This phenomenon occurs when zirconia is exposed to environments of humidity and temperatures between 20-300°C; these conditions lead to a spontaneous transformation from tetragonal (t) phase to monoclinic (m) phase in the material structure [18].…”
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