Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process

Abstract

In the present study, Inconel 718 (IN718) superalloy fabricated by laser powder bed fusion (LPBF) has been characterized focusing on the effect of both homogenization and solution treatment time on grains structure, crystallographic texture, precipitates formation/dissolution and material hardness. For this purpose, a heat-treatment time window with a wide range of soaking times for both treatments was established aiming to develop the optimal post-treatment conditions for laser powder bed fused IN718. It was found that the as-printed IN718 is characterized by very fine columnar/cellular dendrites with Laves phase precipitating at the grain boundaries as well as inter-dendritic regions, which differs from the microstructure of wrought and cast materials and requires special heat-treatment conditions different from the standard treatments. The results reveal that the relatively short homogenization treatment at 1080 °C for 1 h was not enough to significantly change the as-printed grain structure and completely dissolve the segregates and Laves phase. However, a completely recrystallized IN718 material and more Laves phase dissolution were obtained after homogenization treatment for 4 h. A further increase in time of the homogenization treatment (7 h) resulted in grain growth and coarsening of carbides precipitates. The solution treatment time at 980 °C did not cause noticeable changes in the crystallographic texture and grain structure. Nevertheless, the amount of δ-phase precipitation was significantly affected by the solution treatment time. After applying the heat-treatment time window, the hardness increased by 51–72% of the as-printed condition depending on the treatment time due to the formation of γ′ and γ″ in the γ-matrix. The highest material hardness was obtained after 1 h homogenization, whereas the prolonged time treatments reduced the hardness. This study provides a comprehensive investigation of the post heat-treatments of the laser powder bed fused IN718 that can result in an optimized microstructure and mechanical behavior for particular applications.

Effect of homogenization and solution treatments time on the elevated-temperature mechanical behavior of Inconel 718 fabricated by laser powder bed fusion

“…This is attributed to dramatic differences in the initial microstructure obtained after the LPBF, casting and forging manufacturing methods. In our previous study 24 , a post-heat treatment time window covering a wide range of soaking times for the homogenization (from 1 to 7 h at 1080 °C) and solution (from 15 to 60 min at 980 °C) treatments was established, and the effects of these post-treatment conditions on the microstructure, material texture, precipitates and hardness were studied. The objective of that study 24 was to tune the homogenization and solution treatment times to improve the microstructure of LPBF IN718 components, with the ultimate goal of optimizing their mechanical properties.…”

“…In our previous study 24 , a post-heat treatment time window covering a wide range of soaking times for the homogenization (from 1 to 7 h at 1080 °C) and solution (from 15 to 60 min at 980 °C) treatments was established, and the effects of these post-treatment conditions on the microstructure, material texture, precipitates and hardness were studied. The objective of that study 24 was to tune the homogenization and solution treatment times to improve the microstructure of LPBF IN718 components, with the ultimate goal of optimizing their mechanical properties. It was found that after the homogenization treatment for 1 h at 1080 °C, Laves phases and elemental segregation formed during the printing process were not completely dissolved, and the as-printed texture and grain structure were not significantly affected 24 .…”

“…The objective of that study 24 was to tune the homogenization and solution treatment times to improve the microstructure of LPBF IN718 components, with the ultimate goal of optimizing their mechanical properties. It was found that after the homogenization treatment for 1 h at 1080 °C, Laves phases and elemental segregation formed during the printing process were not completely dissolved, and the as-printed texture and grain structure were not significantly affected 24 . However, an increase in the homogenization treatment time at 1080 °C significantly influenced the microstructure in terms of precipitates and texture 24 , and the longer the duration of this treatment, the more intensive the dissolution of Laves phase, the diffusion of segregates and texture weakening 24 .…”

“…It was found that after the homogenization treatment for 1 h at 1080 °C, Laves phases and elemental segregation formed during the printing process were not completely dissolved, and the as-printed texture and grain structure were not significantly affected 24 . However, an increase in the homogenization treatment time at 1080 °C significantly influenced the microstructure in terms of precipitates and texture 24 , and the longer the duration of this treatment, the more intensive the dissolution of Laves phase, the diffusion of segregates and texture weakening 24 . A completely recrystallized material and stress-relieved equiaxed grains were obtained after 4 h of homogenization treatment at 1080 °C 24 .…”

“…However, an increase in the homogenization treatment time at 1080 °C significantly influenced the microstructure in terms of precipitates and texture 24 , and the longer the duration of this treatment, the more intensive the dissolution of Laves phase, the diffusion of segregates and texture weakening 24 . A completely recrystallized material and stress-relieved equiaxed grains were obtained after 4 h of homogenization treatment at 1080 °C 24 . From a negative perspective, more and coarser carbides were observed after the 4 and 7 h homogenization times at 1080 °C 24 .…”