1995
DOI: 10.1051/mmm:1995135
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Influence of Experimental Parameters on the Determination of Tetragonal Distortion in Heterostructures by LACBED

Abstract: Abstract. 2014 The LACBED technique has been applied to the determination of the tetragonal distortion in Si1-xGex/Si heterostructures, which are of great interest in the device technology. The strain determination has been performed on plan sections in an analytical electron microscope. The agreement between this strain value and the tetragonal distortion is influenced mainly by the local sample flatness and the acceleration voltage.Microsc. Microanal. Microstruct. ClassificationPhysics Abstracts 68

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Cited by 9 publications
(3 citation statements)
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“…Two different kinds of MD have been experimentally evidenced by high-resolution electron microscopy (HREM) analyses [10] on the two nominal orientations Si (111) and Si(001): a 90 • Shockley partial (a/6) 112 dislocation and an undissociated (a/2) 110 dislocation respectively. Let us first compare the experimental (h exp -) and theoretical (h cr -) values on the two orientations (001) and (111) in the case of Si 0.7 Ge 0.3 (m = 1.2%) grown at 600 • C. The calculated values are h cr ∼ 8 nm and ∼12 nm on (001) and ( 111) respectively while the experimental values are found to be much larger: h exp 50 nm) [8], and approximately the same on the two orientations. These discrepancies between theoretical predictions and experimental results are explained by the kinetic barrier to dislocation nucleation: in the MB model, MDs nucleate from the propagation of threading dislocations already present in the substrate while in the experiments they nucleate in the epitaxial film on point defects.…”
Section: Plastic Relaxationmentioning
confidence: 93%
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“…Two different kinds of MD have been experimentally evidenced by high-resolution electron microscopy (HREM) analyses [10] on the two nominal orientations Si (111) and Si(001): a 90 • Shockley partial (a/6) 112 dislocation and an undissociated (a/2) 110 dislocation respectively. Let us first compare the experimental (h exp -) and theoretical (h cr -) values on the two orientations (001) and (111) in the case of Si 0.7 Ge 0.3 (m = 1.2%) grown at 600 • C. The calculated values are h cr ∼ 8 nm and ∼12 nm on (001) and ( 111) respectively while the experimental values are found to be much larger: h exp 50 nm) [8], and approximately the same on the two orientations. These discrepancies between theoretical predictions and experimental results are explained by the kinetic barrier to dislocation nucleation: in the MB model, MDs nucleate from the propagation of threading dislocations already present in the substrate while in the experiments they nucleate in the epitaxial film on point defects.…”
Section: Plastic Relaxationmentioning
confidence: 93%
“…The tetragonal distortion can be observed as a splitting of Bragg contours relative to crystallographic planes inclined at an angle with respect to the substrate plane. The tetragonal distortion (ε ⊥ ) may then be deduced from the relative rotation (θ r ) of the planes via [8]…”
Section: Highly Strained Structuresmentioning
confidence: 99%
“…Therefore, it is difficult to measure the strain field of a recent device by a conventional method. [9][10][11][12][13] Recently, it is believed that the origin of split HOLZ lines is the bending of crystals in regions close to interfaces, 5) or crystalline inhomogeneities in the stress layer. 14) Discussion in almost all previous reports on these effects has been based on comparison with a dynamical simulation.…”
mentioning
confidence: 99%