“…Typically, the estimation of the shape and size of nanoparticles has been done using techniques such as atomic force microscopy (AFM), scanning tunneling microscopy (STM), transmission electron microscopy (TEM), and reflection high-energy electron diffraction (RHEED). − These techniques provide the image of a small piece of the sample, and this means that they give information about local properties by characterizing a few nanoparticles at a time. Different shapes of nanoparticles have been reported with the use of these techniques, such as spheres, spheroids, lens-shaped, cone-shaped, pyramids with different facets, truncated pyramids, and different types of polyhedra. ,− A vast amount of information has been obtained through these “structural-characterization techniques”; however, they still have some limitations.…”