In Vitro Behaviour of New Experimental Adhesive Systems

Abstract

Bonding of current adhesives to dentin is usually through the formation of the interfacial hybrid layer between adhesives and dentin. Intertubular and intra-tubular resin infiltration leads to an increase of the quality regarding the dentinal adhesion. The aim of this study is in vitro testing of new experimental adhesives in comparison with commercial adhesive, regarding sorption and solubility as well as to investigate molecular chemical features of the adhesive/dentin interfaces. We used 4 experimental adhesives systems A1, A2, A3, A4 and IBond® (Heraeus) as reference material. Organic phase adhesive system consists of a mixture of monomers. As filler for these systems, besides hydroxyapatite, we used TiO2 nanoparticles. FTIR spectroscopy was used to investigate molecular chemical features of the adhesive/dentin interfaces. The obtained data show the main advantages and disadvantages of the tested adhesive systems. The best values of water sorption and solubility both in water and artificial saliva present A2 and A3 adhesives.

Remineralization products effect on human enamel in vitro study

“…Maximum absorption rates at 1650 cm − 1 , 1540 cm -1 and 1450 cm -1 can be assigned to amide I and amide II bands from the proteins found the enamel structure, with C=O and N-H vibrations. In addition, another large absorption band detected at 3700-3000 cm -1 was assigned to hydroxyl group (O-H) with a secondary band at 1640 cm -1 , which may overlap over amine I bands [19,20].…”