Abstract:High-performance,
high-reliability microelectronic devices are
essential for many applications. Thermal management is required to
ensure that the temperature of semiconductor devices remains in a
safe operating range. Advanced materials, such as silver-sintered
die attach (the bond layer between the semiconductor die and the heat
sink) and metal-diamond composite heat sinks, are being developed
for this purpose. These are typically multilayered structures, with
individual layer thicknesses ranging from tens of… Show more
“…. 23,29 Here, the sample surface is coated with a 10 nm chromium (Cr) adhesion layer and a 150 nm gold transducer layer prior to the FDTR measurement. The high thermoreflectance coefficient of gold (CTR = 2.3 × 10 −4 K −1 ) at the chosen 520 nm probe laser ensures a high measurement sensitivity.…”
Section: ■ Experimental Detailsmentioning
confidence: 99%
“…Measured phase versus frequency results are analyzed by using the n-layer 2D axisymmetric heat diffusion model. 25,29 Clad Metal-Diamond Composite Measurements. Three different clad metal-diamond composite samples were measured by using FDTR.…”
High thermal conductivity
and an appropriate coefficient of thermal
expansion are the key features of a perfect heat spreader for electronic
device packaging, especially for applications with increased power
density and the increasing demand for higher reliability and semiconductor
device performance. For the past decade, metal-diamond composites
have been thoroughly studied as a heat spreader, thanks to their high
thermal conductivities and tailored coefficients of thermal expansion.
While existing thermal characterization methods are good for quality
control purposes, a more accurate method is needed to determine detailed
thermal properties of these composite materials, especially if clad
with metal. Low-frequency-range-domain thermoreflectance has been
adopted to measure the thermal conductivity of a metal-diamond composite
sandwiched between metal cladding layers. Due to this technique’s
low modulation frequencies, from 10 Hz to 10 kHz, multiple layers
can be probed and measured at depths ranging from tens of micrometers
to a few millimeters.
“…. 23,29 Here, the sample surface is coated with a 10 nm chromium (Cr) adhesion layer and a 150 nm gold transducer layer prior to the FDTR measurement. The high thermoreflectance coefficient of gold (CTR = 2.3 × 10 −4 K −1 ) at the chosen 520 nm probe laser ensures a high measurement sensitivity.…”
Section: ■ Experimental Detailsmentioning
confidence: 99%
“…Measured phase versus frequency results are analyzed by using the n-layer 2D axisymmetric heat diffusion model. 25,29 Clad Metal-Diamond Composite Measurements. Three different clad metal-diamond composite samples were measured by using FDTR.…”
High thermal conductivity
and an appropriate coefficient of thermal
expansion are the key features of a perfect heat spreader for electronic
device packaging, especially for applications with increased power
density and the increasing demand for higher reliability and semiconductor
device performance. For the past decade, metal-diamond composites
have been thoroughly studied as a heat spreader, thanks to their high
thermal conductivities and tailored coefficients of thermal expansion.
While existing thermal characterization methods are good for quality
control purposes, a more accurate method is needed to determine detailed
thermal properties of these composite materials, especially if clad
with metal. Low-frequency-range-domain thermoreflectance has been
adopted to measure the thermal conductivity of a metal-diamond composite
sandwiched between metal cladding layers. Due to this technique’s
low modulation frequencies, from 10 Hz to 10 kHz, multiple layers
can be probed and measured at depths ranging from tens of micrometers
to a few millimeters.
“…Thermal conductivity and thermal boundary conductance (TBC) of multilayers have been widely characterized with the optical pump–probe thermoreflectance techniques. , The traditional thermoreflectance methods, such as time-domain thermoreflectance (TDTR) and frequency-domain thermoreflectance (FDTR), have shallow thermal penetration depths (∼0.2 to 3 μm) under standard operating conditions. , Therefore, only the part of the sample near the sample surface can be probed, leading to the poor sensitivity of measuring deeply buried layers and interfaces. The recently reported steady-state thermoreflectance (SSTR) , and low-frequency FDTR methods have been demonstrated for the measurement of buried layers and interfaces. For the SSTR, intentionally controlling the pump spot size can extend the thermal penetration depth to tens of micrometers, maximizing the measurement sensitivity for the target properties of the buried layers and interfaces .…”
Section: Introductionmentioning
confidence: 99%
“…For the SSTR, intentionally controlling the pump spot size can extend the thermal penetration depth to tens of micrometers, maximizing the measurement sensitivity for the target properties of the buried layers and interfaces . For the low-frequency FDTR, measuring from 10 Hz to 10 kHz enables multiple layers to be probed at depths from tens of micrometers to millimeters . Although thermal characterization of deeply buried layers was achieved by the recently developed methods, the pump–probe thermoreflectance methods are often limited for the challenge of simultaneously extracting the multiple unknown parameters when characterizing the multilayer structure .…”
Section: Introductionmentioning
confidence: 99%
“…Although thermal characterization of deeply buried layers was achieved by the recently developed methods, the pump–probe thermoreflectance methods are often limited for the challenge of simultaneously extracting the multiple unknown parameters when characterizing the multilayer structure . To measure the GaN HEMT structure, investigated in the study, with the traditional thermoreflectance methods where a metal transducer is routinely deposited on the sample surface, ,,− at least five parameters (TBC at metal transducer/GaN interface, thermal conductivity of undoped GaN, thermal conductivity of doped GaN buffer, TBC at GaN/substrate interface, and substrate thermal conductivity) need to be extracted simultaneously in the fitting. The large number of fitting parameters limits the measurement accuracy.…”
Measuring the thermal properties of the buried GaN buffer layer and interface in GaN high-electron mobility transistor (HEMT) structures is of crucial importance. This remains challenging with the traditional pump−probe thermoreflectance techniques due to their limited thermal penetration depths and the difficulty in extracting the large number of unknown parameters in the multilayer HEMT structure. This work applies a transducer-less transient thermoreflectance technique (TL-TTR) for the characterization. We experimentally and numerically investigate the dynamic thermal transport process of the TL-TTR measurement, benchmarking against that of the traditional metal transducer transient thermoreflectance (MT-TTR) measurement. The significantly different heat absorption and dissipation processes in the two measurements lead to the distinctive measurement sensitivities. Notably, the sensitivity of TL-TTR signal to all unknown thermal properties follows a distinctive trend over the measurement time region, demonstrating the technique's capability of measuring the buried buffer thermal conductivity and the thermal boundary conductance (TBC) across the buffer/substrate interface. This is illustrated by measuring three different GaN-on-SiC wafers with highly Fe-doped buffer layers. The uncertainties of buffer thermal conductivity and TBC, determined by TL-TTR, are as low as ±6 and ±13%, respectively. In contrast, MT-TTR measures the buffer thermal conductivity and TBC with the uncertainties as large as ±20 and ±30%. The TL-TTR technique enables a non-invasive platform to characterize the thermal properties of the advanced GaN-based materials with complex structures and achieve a more in-depth understanding the phonon transport mechanisms.
The thermoreflectance technique is one of the few methods which can measure thermal diffusivity of thin films as thin as 100 nm or thinner in the cross-plane direction. The thermoreflectance method under rear-heat front-detect configuration is sometimes called ultrafast laser flash method because of its similarity to laser flash method. Up to now it has typically only been possible to attempt to evaluate the interfacial thermal resistance between the thin films by preparing and measuring several samples with different thicknesses. In this study, a method to directly determine interfacial thermal resistance by a single measurement of a thin film on substrate is represented, by analyzing the shape of thermoreflectance signals with analytical solutions in frequency domain and time domain. Thermoreflectance signals observed from metallic thin films on sapphire substrate with different thickness steps were analyzed by Fourier analysis and fitted by analytical equations with four parameters: heat diffusion time across the first layer, ratio of virtual heat sources, characteristic time of cooling determined by interfacial thermal resistance and relative amplitude of the signal. Interface thermal resistance between the thin film and substrate was able to be determined reliably with smaller uncertainty.
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