In Operando Study of Microsupercapacitors with Gel Electrolytes Using Nano‐Beam Synchrotron X‐ray Diffraction
Gui Li,
Nicolas Boulanger,
Artem Iakunkov
et al.
Abstract:Synchrotron radiation X‐ray diffraction (XRD) with nanoscale beam size was used here for in situ and in operando study of micro‐supercapacitors (MSC) with gel electrolyte and MXene Ti3C2Tx electrodes. The electrode structure was characterized as a function of applied voltage and distance from the gap separating electrodes using microscopic cells with cylindrical shape designed for transmission mode XRD. The devices with gel electrolytes based on H2SO4 (with H2O/PVA and DMSO/PVA) showed stable performance with … Show more
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