Imidazoles. XII. Synthesis of substituted benzylthioalkylimidazolines

Iradyan, M. A.; Aroyan, R. A.; Ktsoyan, L. A.; Aroyan, A. A.

doi:10.1007/bf01156479

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“…Firstly, compound 1 , ethylimido‐ p ‐bromophenylacetate hydrochloride, was prepared according to the Pinner method (Scheme ).…”

Section: Resultsmentioning

confidence: 99%

Microwave‐Assisted Synthesis of Some Novel Benzimidazole Derivatives Containing Imine Function and Evaluation of Their Antimicrobial Activity

Kahveci

Yılmaz

Menteşe

et al. 2013

Journal of Heterocyclic Chem

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in Wiley Online Library (wileyonlinelibrary.com). NH 2 + OEt Br Cl -Br NH 2 NH 2 + N N O NH N Br Br Ar 5a-k 2 N N H Br Br4-Bromo-o-phenylenediamine and ethylimido-p-bromophenylacetate, 1, were subjected to microwave irradiation to synthesize benzimidazole derivative, compound 2. Ester derivative, 3, and hydrazide derivative, 4, of compound 2 were also synthesized, respectively. Finally, compound 4 was treated with 11 different aromatic aldehydes to obtain benzimidazole derivatives containing imine function. All reactions were carried out with microwave irradiation and conventional heating, and results were compared. Some of the newly synthesized compounds showed moderate antimicrobial activity against some tested organisms.

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“…Firstly, compound 1 , ethylimido‐ p ‐bromophenylacetate hydrochloride, was prepared according to the Pinner method (Scheme ).…”

Section: Resultsmentioning

confidence: 99%

Microwave‐Assisted Synthesis of Some Novel Benzimidazole Derivatives Containing Imine Function and Evaluation of Their Antimicrobial Activity

Kahveci

Yılmaz

Menteşe

et al. 2013

Journal of Heterocyclic Chem

View full text Add to dashboard Cite

show abstract

“…Imidazolinylhydrazone is unstable to electron impact [3]. Decomposition of the synthesized hydrazones, which occurs with elimination of the methyl radical, NO, NO 2 , and alkyl from [M] + , was studied using XX as an example.…”

mentioning

confidence: 99%