Shedding Light on Electrocatalysts: Practical Considerations for Operando Studies with High‐Energy X‐Rays
Rebecca K. Pittkowski
Abstract:Operando studies using high‐energy X‐rays from synchrotron sources are essential for unraveling the complex material transformation that electrocatalysts undergo under operating conditions. This article explores key considerations to perform these experiments and the insights gained from such studies on nanostructured electrocatalysts. Critical factors include optimizing electrochemical performance while obtaining high‐quality X‐ray signals, which often require compromises. The electrochemical operando cell de… Show more
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