In situ Investigations of the Formation Mechanism of Metastable γ‐BiPd Nanoparticles in Polyol Reductions
Matthias Smuda,
Noah Elsner,
Jonas Ströh
et al.
Abstract:Synthesizing intermetallic phases containing noble metals often poses a challenge as the melting points of noble metals often exceed the boiling point of bismuth (1560 °C). Reactions in the solid state generally circumvent this issue but are extremely time consuming. A convenient method to overcome these obstacles is the co‐reduction of metal salts in polyols, which can be performed within hours at moderate temperatures and even allows access to metastable phases. However, little attention has been paid to the… Show more
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