Hydrolysis and Alcoholysis of 2,3-Dichlorodioxane.

Salomaa, Pentti; Schotte, Lennart; Vihovde, E. Hadler; Sørensen, Nils Andreas

doi:10.3891/acta.chem.scand.08-0744

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1972

1975

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“…Thermolysis of (-) --Chlorobenzyl 2(E)-Octyl Ether. A preliminary thermolysis of (-) -a -chlorobenzyl 2(ff)-octyl ether (4) in sulfolane in which only low-boiling products were collected gave 2-octene: NMR 5.40 (m, 2 H, -CHCH-), 2.30-0.70 (m, aliphatic H). (An excellent comparison with Sadtler spectrum no.…”

Section: Resultsmentioning

confidence: 99%

“…The ratios of the triplet to singlet and singlet to CHO from butyraldehyde were 1:1 and 6:1, respectively (25% reaction). An interesting point to note is that the condensation, eq 5, was so much faster in the presence of 5 than when CRCRCRCHOCR -* CRC1 + CRCRCRCHO (4) Cl 5 2CRCRCRCHO CRCRCH2CH=C-CHO + RO (5) C2R butyraldehyde was thermolyzed alone. This can be explained by acid catalysis.…”

Section: Resultsmentioning

confidence: 99%

“…[a]24D -36.8°( CCL); NMR (CCL) 7.39 (m, 5 H, phenyl), 6.58 (s, 1 H, OCHC1), 4.05 (m, 1 H, OCH), 1.90-0.60 (complex m, 16 H, aliphatic H). Anal.…”

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confidence: 99%

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