Abstract:Different ratios of octavinylsilsesquioxane (OVS) reacted with phenyl‐substituted double‐decker silsesquioxane (Ph‐DDSQ) via the simple Friedel‐Crafts reaction provides several innovative silsesquioxane‐based porous polymers (PCS‐ODs). The hybrid polymers show adjustable porosity (specific surface areas of 1235 m2 g−1 and large pore volumes >1.07 cm3 g−1). FTIR, SEM, BET, TGA, solid‐state 13C and 29Si MAS NMR spectra were employed to fully characterize these hybrid materials. They display good adsorption ca… Show more
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