HPLC-MS/MS analysis of 9 artificial sweeteners in imported foods

Lim, Ho-Soo; Park, Sung-Kwan; Kwak, In-Shin; Kim, Hyung-Il; Sung, Jun-Hyun; Jang, Su-Jin; Byun, Mi-Youn; Kim, So-Hee

doi:10.1007/s10068-013-0072-2

Cited by 27 publications

(13 citation statements)

References 15 publications

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“…LLE involves addition of an organic solvent to the food in liquid form. Sweeteners are then extracted from the liquid aqueous phase into the organic phase [6]. Solid-liquid extraction (SLE) is the process of partitioning target analytes from a solid state into a solvent prior to dilution and filtration.…”

Section: Sample Preparationmentioning

confidence: 99%

“…Huang et al used tiopronin as the internal standard for the determination of CYC in foods using ionpair HPLC coupled to ESI-MS [21]. Sodium warfarin has been used as an internal standard in previous multi-sweetener methods for determination of several target analytes [5,6]. Sucralose-d6 was used as the internal standard for the determination of SCL by ESI-LC/MS-MS in waste and surface waters [8].…”

Section: Internal Standardsmentioning

confidence: 99%

“…Nine sweeteners were determined in foods using HPLC ESI-MS/MS in multiple reaction monitoring mode (MRM) with improved MS confirma-fi tion data [6]. Analytes were separated on a Th ermo Hypersil BPS C18 colTh umn (250 × 3 mm, 5 μm).…”

Section: Hplc-ms/tandem Ms Detectionmentioning

confidence: 99%

“…The list of allowable sweeteners varies among nations worldwide [5]. Th For example, CYC and NHDC are not approved for use as food additives by the US Food and Drug Administration (FDA) but are authorized in the European Union (EU) [6].…”

Section: Introductionmentioning

confidence: 99%

See 3 more Smart Citations

Recent Analytical Methods for the Analysis of Sweeteners in Food: A Regulatory Perspective

Shah

Jager

2016

Food Safety

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Section: Sample Preparationmentioning

confidence: 99%

Section: Internal Standardsmentioning

confidence: 99%

Section: Hplc-ms/tandem Ms Detectionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

See 2 more Smart Citations

Recent Analytical Methods for the Analysis of Sweeteners in Food: A Regulatory Perspective

Shah

Jager

2016

Food Safety

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“…There have been reports that the excessive use of saccharin sodium will cause cancer. Various methods including high performance liquid chromatography (HPLC), capillary zone electrophoresis (CZE), and thin layer chromatography have been proposed for the determination of saccharin sodium [20][21][22][23][24][25][26][27][28][29][30]. Instead of these methods, developing a cost-effective saccharin sodium imprinted polymer under water-compatible medium will prove to be a more realistic option for separation and purification of saccharin sodium as well as for its specific and selective measurement in its formulated products.…”

Section: Introductionmentioning

confidence: 99%

Water-compatible surface imprinting of ‘Saccharin sodium’ on silica surface for selective recognition and detection in aqueous solution

Song

Yang

Zhao

et al. 2015

Talanta

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Voltammetric Determination of Neotame by Using Chitosan/Nickelnanoparticles/Multi Walled Carbon Nanotubes Biocomposite as a Modifier

İncebay

Saylakcı

2021

Electroanalysis

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A selective and simple biosensor was prepared by immobilizing chitosan/nickelnanoparticles/multi‐walled carbon nanotubes biocomposite on the glassy carbon electrode surface for voltammetric quantification of neotame. The properties and morphology of the modified electrode surfaces were characterized by scanning electron microscope (SEM), energy dispersive X‐ray analysis (EDX). Electro oxidation of neotame on this modified surface was examined through cyclic voltammetry (CV) and square wave voltammetry (SWV) techniques. The biocomposite modified surface (Chi/NiNPs/MWCNTs/GCE) proposed in this study showed good electrocatalytic activity for neotame with an improved voltammetric peak current at 1.004 V, unlike the bare glassy carbon electrode (GCE) surface and several other modified surfaces. Under optimum conditions, Chi/NiNPs/MWCNTs/GCE gave linear SWV responses at the range of 2 μM ∼50 μM for neotame with 0.84 μM determination limit. This voltammetric sensor was successfully employed for the quantification of neotame on food samples and showed long‐term stability, advanced voltammetric behavior, and good repeatability. Selective, accurate, and precise determination of neotame highlight the importance of this electrode in monitoring the control of food additives and ensures attract a great deal of attention.

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HPLC-MS/MS analysis of 9 artificial sweeteners in imported foods

Cited by 27 publications

References 15 publications

Recent Analytical Methods for the Analysis of Sweeteners in Food: A Regulatory Perspective

Recent Analytical Methods for the Analysis of Sweeteners in Food: A Regulatory Perspective

Water-compatible surface imprinting of ‘Saccharin sodium’ on silica surface for selective recognition and detection in aqueous solution

Voltammetric Determination of Neotame by Using Chitosan/Nickelnanoparticles/Multi Walled Carbon Nanotubes Biocomposite as a Modifier

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