How does the order of sample analysis influence the matrix effect during LC-MS bioanalysis?

Gniazdowska, Elżbieta; Giebułtowicz, Joanna; Rudzki, Piotr J.

doi:10.1016/j.jchromb.2023.123800

Cited by 5 publications

(2 citation statements)

References 39 publications

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“…This study was overcome by calibrating instruments using substrate fortification criteria but with low recovery rates of 68–82%. The solid-phase extraction, isotope internal standardization, dilution, protein precipitation, and other strategies can be used to reduce the matrix effect and improve the recovery rates.…”

Section: Detection Of Gizzerosinementioning

confidence: 99%

Formation and Detection of Gizzerosine in Animal Feed Matrices: Progress and Perspectives

Jiao,

Qian

et al. 2024

J. Agric. Food Chem.

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Gizzerosine is responsible for gizzard erosion and black vomit, owing to excessive gastric acid secretion in poultry. It is a biogenic amine that forms during feed processing. Gizzerosine, a derivative of histamine, is a serious threat to animal feed safety and poultry production because it is more potent after ingestion and more harmful to poultry than histamine. The difficulty of obtaining gizzerosine and the lack of simple, rapid, and sensitive in vitro detection techniques have hindered studies on the effects of gizzerosine on gizzard health and poultry production. In this review, we evaluated the natural formation and the chemical synthesis methods of gizzerosine and introduced seven detection methods and their principles for analyzing gizzerosine. This review summarizes the issues of gizzerosine research and suggests methods for the future development of gizzerosine detection methods.

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Section: Detection Of Gizzerosinementioning

confidence: 99%

Formation and Detection of Gizzerosine in Animal Feed Matrices: Progress and Perspectives

Jiao,

Qian

et al. 2024

J. Agric. Food Chem.

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“…Cortese i współpracownicy opisują wszystkie metody określania wpływu matrycy i sposoby jego korygowania [22]. Zaskoczeniem jest także możliwość wykorzystania jedynie 1 osocza lipemicznego, którego zróżnicowanie w zawartości składników matrycy jest bardzo duże pomiędzy różnymi źródłami [23] i według przeprowadzonych badań [24].…”

Section: Dyskusja I Podsumowanieunclassified

ICH M10 guideline - a harmonized global approach to bioanalysis

Gniazdowska,

Gilant,

Buś-Kwaśnik

2023

Prosp. Pharm. Sc.

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Bioanalytical methods are used in research on small-molecule and large-molecule drug products to determine analytes and their metabolites in biological matrices such as blood, plasma, serum, urine, feces, saliva, other biological fluids, or tissues. Validation of a bioanalytical method is the essential step before the implementation of the method into routine use in toxicokinetic or pharmacokinetic studies. Harmonization of recommendations for the validation of bioanalytical methods has been advocated for many years. In 2022, The International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use (ICH) finished the work on final version of the ICH M10 guideline, as a combination of four regional guidelines (American, European, Brazilian and Japanise). The document uniforms rules for the performance of the bioanalytical method validation and documentation of sample analysis from clinical and non-clinical studies in most countries around the world, which are submitted to registration authorities.

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MonoTip C18 pipette tip solid-phase extraction coupled with liquid chromatography-tandem mass spectrometry enables rapid and automated therapeutic drug monitoring of tyrosine kinase inhibitors

Wang,

Liu,

Zheng

et al. 2024

Arabian Journal of Chemistry

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How does the order of sample analysis influence the matrix effect during LC-MS bioanalysis?

Cited by 5 publications

References 39 publications

Formation and Detection of Gizzerosine in Animal Feed Matrices: Progress and Perspectives

Formation and Detection of Gizzerosine in Animal Feed Matrices: Progress and Perspectives

ICH M10 guideline - a harmonized global approach to bioanalysis

MonoTip C18 pipette tip solid-phase extraction coupled with liquid chromatography-tandem mass spectrometry enables rapid and automated therapeutic drug monitoring of tyrosine kinase inhibitors

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