“…30,31 However, the catalytic performance of NiS 2 in the degradation of organic pollutants such as endocrine disrupting compounds (EDCs) is still less competitive compared to other catalytic materials based on phosphides and noble metals. 4,13 In this regard, numerous techniques have been used to develop and fabricate nickel sulde nanostructures with good physical and chemical properties including hydrothermal methods, 23,32,33 solvothermal, 34 decomposition of single-source precursors, 35 microwave-assisted synthesis, 36,37 solventless route in air, 38 sonochemical, 39 and ultrasonic spray pyrolysis. 10 Most of these methods are suitable for preparing nickel suldes in powder form with other different phases sometimes accompanying.…”