Abstract:Abstract. The use of spherical rotors for magic angle spinning offers a number of advantages including improved sample exchange, efficient microwave coupling for dynamic nuclear polarization nuclear magnetic resonance (NMR) experiments and, most significantly, high frequency and stable spinning with minimal risk of rotor crash. Here we demonstrate the sim- ple retrofitting of a commercial NMR probe with MAS spheres for solid-state NMR. We analyze a series of turbine groove geometries to investigate the importa… Show more
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