2002
DOI: 10.1063/1.1435830
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Highly ordered monocrystalline silver nanowire arrays

Abstract: Highly ordered silver nanowire arrays have been obtained by pulsed electrodeposition in self-ordered porous alumina templates. Homogeneous filling of all the pores of the alumina template is achieved. The interwire distance is about 110 nm corresponding to a density of silver nanowires of 61ϫ10 9 in. Ϫ2 and the diameter can be varied between 30 and 70 nm. The silver wires are monocrystalline with some twin lamella defects and grow perpendicular to the ͗110͘ direction. The previously encountered difficulty to o… Show more

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Cited by 377 publications
(262 citation statements)
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“…36 The deposition pulse was a 6 ms negative potential of Ϫ6 V, followed by a 6 ms positive potential of 6 V and a zero potential with delay time of 400 ms. The length of Ag nanowires was controlled by the deposition integral coulomb charge.…”
Section: Preparation Of Samplesmentioning
confidence: 99%
“…36 The deposition pulse was a 6 ms negative potential of Ϫ6 V, followed by a 6 ms positive potential of 6 V and a zero potential with delay time of 400 ms. The length of Ag nanowires was controlled by the deposition integral coulomb charge.…”
Section: Preparation Of Samplesmentioning
confidence: 99%
“…Previously, alumina membranes obtained from the anodization of thick ͑Ͼ100 m͒ aluminum foils were mostly used for the fabrication of nanowires. [23][24][25][26][27][28][29][30] These nanowires were grown by electrodeposition, which cannot be easily adapted for the fabrication of nanodots with controlled and uniform thickness. Moreover, this method requires transfer of the alumina membranes onto a substrate.…”
Section: Introductionmentioning
confidence: 99%
“…13 Figure 2.1: Pulse parameters used by Sauer et al to yield single crystal silver nanowires. Taken from reference 13 .…”
Section: Electrochemistry Backgroundmentioning
confidence: 99%
“…A potentiostat was used to control the electrochemical reaction performed between the counter, reference, and working (sputtered gold film) electrodes. g/l ammonium citrate was added under the same conditions to adjust the ph of the solution to 4.5 (as reported by reference) 13 . The final silver solution used to deposit nanowires was made by adding 2% Difco gelatin by weight to a commercial silver bath solution, 1025 RTU, made by Technic Inc. Then the solution was diluted with water according to the ratio 1:1.…”
Section: Nanowire Fabricationmentioning
confidence: 99%
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