High‐Yield Synthesis of a New Layered High‐Nuclearity Carbonyl Osmium‐Rhodium Cluster Complex – Synthesis, Structural Characterization, and Electrochemistry of [PPN][Os9Rh3(μ‐CO)2(CO)26]
Abstract:A direct and high-yield synthetic route for a novel dodecanuclear osmium-rhodium mixed-metal cluster is presented. The redox properties of the cluster were examined, and it was found that the anion behaves as an "electron reservoir".
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