Growth and characterization of a new polymorph of lead succinate: A promising NLO material

Dhanya, V.S.; Sudarsanakumar, M.R.; Suma, S.; Prasanna, S.; Babu, K. Rajendra; Kumar, B. Santhosh; Roy, Sunalya M.

doi:10.1016/j.jcrysgro.2011.01.073

Cited by 29 publications

(14 citation statements)

References 25 publications

(35 reference statements)

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“…The absorption bands at 1285 and 927 cm -1 are due to asymmetric and symmetric C-C stretching, respectively. The bending and rocking vibrations of COOare observed at 659 and 523 cm -1 , respectively (Padmanabhan et al 2005;Jianguo Pan et al 2007;Krishnan et al 2007;Dhanya et al 2011).…”

Section: Ft-ir Analysismentioning

confidence: 99%

Growth, characterization and dielectric property studies of gel grown barium succinate single crystals

Binitha

Pradyumnan

2014

Bull Mater Sci

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Single crystals of barium succinate (BaC 4 H 4 O 4) were grown in silica gel medium using controlled chemical reaction method. Plate-like single crystals of size up to 3 × 2 × 0⋅2 mm 3 was obtained. Single crystal X-ray diffraction (XRD) studies confirmed that structure of the title compound is tetragonal. Powder X-ray diffraction (PXRD) pattern of the grown crystal and the Fourier transform infrared (FT-IR) spectrum in the range 400-4000 cm-1 are recorded. The vibrational bands corresponding to different functional groups are assigned. Thermal stability of the grown crystals is confirmed by differential scanning calorimetry (DSC). Dielectric constant and dielectric loss have been calculated and discussed as a function of frequency at different temperatures.

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Section: Ft-ir Analysismentioning

confidence: 99%

Growth, characterization and dielectric property studies of gel grown barium succinate single crystals

Binitha

Pradyumnan

2014

Bull Mater Sci

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“…The absorption band at 1425 cm −1 is due to symmetric stretching vibration of COO-group. 21,22 The absorption bands at 1206 cm −1 and 993 cm −1 are due to asymmetric and symmetric C-C stretching respectively. 23 The FT-IR studies confirm the presence of the expected functional groups in the crystal and support the structure of the crystal.…”

Section: Ft-ir Analysesmentioning

confidence: 99%

“…The relatively high values of dielectric constant at higher frequencies find applications in ferroelectric, photonic and electro-optic devices. 21 Variation of dielectric constant with temperature is generally attributed to the orientational polarization, crystal expansion, the presence of impurities and crystal defects. When temperature increases, the dielectric constant decreases, as evident from the Fig.…”

Section: Electrical Property Studiesmentioning

confidence: 99%

Growth and Studies of Properties of Copper Succinate Dihydrate Single Crystals

Binitha

Pradyumnan

2013

Mod. Phys. Lett. B

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Single crystals of copper succinate dihydrate (CSD) with triclinic structure were grown in silica gel medium. The functional groups in the crystal were analyzed by FT-IR Spectroscopy. Atomic Force Microscopy (AFM) revealed the striations on the surface of grown crystals, which were incorporated during its time of growth. Thermal degradation studies have been carried out by Differential Scanning Calorimetry (DSC). Dielectric constant and AC conductivity have been estimated as a function of frequency at different temperatures.

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“…The absorption bands at 1195 cm -1 and 1069 cm -1 are due to asymmetric and symmetric C-C stretching respectively. The weak band at 719cm -1 represents the absorption of the wagging vibration of the C-H bond in the -CH2 groups [16][17][18] .…”

Section: Figure 4 Ft-ir Spectrum Of Zsmentioning

confidence: 99%

Growth, Characterization and Dielectric Property Studies of Zinc Succinate Crystals Grown in Silica Gel Medium

M.P¹

2012

IOSRJAP

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Growth and characterization of a new polymorph of lead succinate: A promising NLO material

Cited by 29 publications

References 25 publications

Growth, characterization and dielectric property studies of gel grown barium succinate single crystals

Growth, characterization and dielectric property studies of gel grown barium succinate single crystals

Growth and Studies of Properties of Copper Succinate Dihydrate Single Crystals

Growth, Characterization and Dielectric Property Studies of Zinc Succinate Crystals Grown in Silica Gel Medium

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