Fully automated station for testing, characterizing and modifying screen-printed electrodes

Zítka, Jan; Šı́lený, Jan; Kudr, Jiří; Koudelková, Zuzana; Ilieva, Lada; Richtera, Lukáš; Syrový, Tomáš; Adam, Vojtěch; Zítka, Ondřej

doi:10.1039/d2ay01123a

Cited by 3 publications

(3 citation statements)

References 32 publications

(38 reference statements)

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“…This station was accomplished in the system integrated minipotentiostat EmStat 4 (PalmsSens, Houten, The Netherlands) interfaced to station inherent software (Fig. 1 ) [ 36 ]. In the case of electrochemical measurements realized by laboratory operator, potentiostat PalmSens 4 (PalmSesns, Houten, The Netherlands) was used.…”

Section: Methodsmentioning

confidence: 99%

“…Further details are described in Anal. Methods , 2022, 14, 3824 [ 36 ]. All experiments, except for manual real sample analysis and manual modification, were performed using this automated benchtop system.…”

Section: Methodsmentioning

confidence: 99%

“…Our unique approach to high-throughput electrochemistry is based on unique BES and related software that enable facile and reliable electrochemical analysis and individual SPEs processing in fully automatic mode. This approach is in general fully described at [ 36 ] and belongs to our continuous work in this field of electrochemical analysis automation [ 37 , 38 ].…”

Section: Introductionmentioning

confidence: 99%

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Proving the automatic benchtop electrochemical station for the development of dopamine and paracetamol sensors

Haššo,

Kudr,

Zítka

et al. 2024

Microchim Acta

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The introduced work represents an implementation of the automatic benchtop electrochemical station (BES) as an effective tool for the possibilities of high-throughput preparation of modified sensor/biosensors, speeding up the development of the analytical method, and automation of the analytical procedure for the determination of paracetamol (PAR) and dopamine (DOP) as target analytes. Within the preparation of gold nanoparticles modified screen-printed carbon electrode (AuNPs-SPCE) by electrodeposition, the deposition potential EDEP, the deposition time tDEP, and the concentration of HAuCl4 were optimized and their influence was monitored on 1 mM [Ru(NH3)6]3+/2+ redox probe and 50 μM DOP. The morphology of the AuNPs-SPCE prepared at various modification conditions was observed by SEM. The analytical performance of the AuNPs-SPCE prepared at different modification conditions was evaluated by a construction of the calibration curves of DOP and PAR. SPCE and AuNPs-SPCE at modification condition providing the best sensitivity to PAR and DOP, were successfully used to determine PAR and DOP in tap water by “spike-recovery” approach. The BES yields better reproducibility of the preparation of AuNPs-SPCE (RSD = 3.0%) in comparison with the case when AuNPs-SPCE was prepared manually by highly skilled laboratory operator (RSD = 7.0%). Graphical abstract

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Section: Methodsmentioning

confidence: 99%

Section: Methodsmentioning

confidence: 99%