1985
DOI: 10.1093/elt/39.1.63-b
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From Jonathan Seath

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“…Addition of 5 mol% CySH was sufficient to reduce oligomeric byproducts that arise from slow HAT and provide synthetically useful yields across a broad range of alkene subtypes (Scheme 5, 3f-i). 29 This subtle addition allowed for the effective use of alkenes substituted with halides (F, Cl, Br), providing a novel route towards compounds typically accessed through elimination prone nucleophilic displacement. Vinyl metalloids and main group elements were readily incorporated, β-boryl, silyl and phosphoryl pyridines could be forged in this manner in a single synthetic step.…”
Section: Radical Hydroarylation Of Neutral and Rich Olefinsmentioning
confidence: 99%
“…Addition of 5 mol% CySH was sufficient to reduce oligomeric byproducts that arise from slow HAT and provide synthetically useful yields across a broad range of alkene subtypes (Scheme 5, 3f-i). 29 This subtle addition allowed for the effective use of alkenes substituted with halides (F, Cl, Br), providing a novel route towards compounds typically accessed through elimination prone nucleophilic displacement. Vinyl metalloids and main group elements were readily incorporated, β-boryl, silyl and phosphoryl pyridines could be forged in this manner in a single synthetic step.…”
Section: Radical Hydroarylation Of Neutral and Rich Olefinsmentioning
confidence: 99%