2013
DOI: 10.2324/ejsm.9.1
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Free-radical polymerization of tetraethyl (2,3-dimethylenebutane-1,4-diyl)bis(phosphonate)

Abstract: Free-radical polymerization of tetraethyl (2,3-dimethylenebutane-1,4-diyl)bis(phosphonate), a 1,3-butadiene derivative containing two diethyl phosphonate functions in a molecule, was carried out under various conditions. When polymerization was performed in benzene at 60 C for 21 h with using 1 mol% of 2,2-azobisisobutyronitrile as an initiator, sticky polymer was obtained in 70% yield without forming gel. Number average molecular weight of the polymer thus obtained was estimated to be 69,000 by SEC based on p… Show more

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