Fluorination of 5′-deoxy-5′-(methylthio)adenosine with xenon difluoride provides an expedient synthesis of (fluoromethylthio)adenosine

Guillerm, Georges; Gâtel, Marie

doi:10.1039/p19940000153

Cited by 6 publications

(1 citation statement)

References 14 publications

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“…A convenient method for the synthesis of 5 H -(fluoromethylthio)adenosine derivatives (242) (yield 70%) by regioselective fluorination of 5-methylthioadenosine derivatives 243 by XeF 2 has been proposed. 397 In this case, as in the fluorination of the 392 and biotin derivatives, 394 the reaction occurs at the least substituted carbon atom.…”

Section: Xef2mentioning

confidence: 99%

Chemistry of xenon derivatives. Synthesis and chemical properties

Brel¹,

Pirkuliev²,

Зефиров³

2001

Russ. Chem. Rev.

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The critical relaxation of the four-state Potts model on L x L lattices with L 5 64 is studied by the Monte Carlo method. The decay of the magnetisation from a nonequilibrium initial state exhibits a crossover from a power-law relaxation for I<< r ' ( L ) to an exponential one for r > > f ' ( L ) ,where t ' ( L ) is some crossover time. This crossover is discussed within the context of dynamic finite-size scaling theory. As a result, the dynamic critical exponent is estimated to be Z = 2.94 * 0.29.

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Section: Xef2mentioning

confidence: 99%

Chemistry of xenon derivatives. Synthesis and chemical properties

Brel¹,

Pirkuliev²,

Зефиров³

2001

Russ. Chem. Rev.

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ChemInform Abstract: Fluorination of 5′‐Deoxy‐5′‐(methylthio)adenosine with Xenon Difluoride Provides an Expedient Synthesis of (Fluoromethylthio) adenosine (V).

Guillerm

Gâtel

1994

ChemInform

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Fluorination of 5'-Deoxy-5'-(methylthio)adenosine with Xenon Difluoride Provides an Expedient Synthesis of (Fluoromethylthio) adenosine (V). -Preliminary investigations with regard to the biological activity of ( V) as a potential inhibitor of typical bacterial enzymes show that (V) inhibits 5'-methylthioadenosine nucleosidase from E. coli. -(GUILLERM, G.; GATEL, M.; J. Chem. Soc., Perkin Trans. I (1994) 2, 153-154; Lab. Chim.

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Xenon difluoride in synthesis

Tius

1995

Tetrahedron

168

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Fluorination of 5′-deoxy-5′-(methylthio)adenosine with xenon difluoride provides an expedient synthesis of (fluoromethylthio)adenosine

Cited by 6 publications

References 14 publications

Chemistry of xenon derivatives. Synthesis and chemical properties

Chemistry of xenon derivatives. Synthesis and chemical properties

ChemInform Abstract: Fluorination of 5′‐Deoxy‐5′‐(methylthio)adenosine with Xenon Difluoride Provides an Expedient Synthesis of (Fluoromethylthio) adenosine (V).

Xenon difluoride in synthesis

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