1991
DOI: 10.1016/s0022-1139(00)81249-x
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Fluorinated amino acids and peptides. Synthesis of 3,3-difluoro-2-amino acids, peptides and cyclodipeptides incorporating 3,3-difluoro-2-aminobutyric acid or 3,3-difluorophenylalanine residues in their structures

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Cited by 3 publications
(1 citation statement)
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“…A slight modification to the original procedure, adding PPh 3 first and leaving to stir for 5 h before adding water, increased the yield to 93%. Fmoc protection to give 18 was followed by removal of the tert -butyl group to give the desired lipophilic amino acid Fmoc-Laa 4 in 46% overall yield from 11 .…”
Section: Resultsmentioning
confidence: 99%
“…A slight modification to the original procedure, adding PPh 3 first and leaving to stir for 5 h before adding water, increased the yield to 93%. Fmoc protection to give 18 was followed by removal of the tert -butyl group to give the desired lipophilic amino acid Fmoc-Laa 4 in 46% overall yield from 11 .…”
Section: Resultsmentioning
confidence: 99%