Poisson's spot is a diffraction phenomenon producing an intensity maximum at the center of the geometric shadow of circular opaque objects. In an analog of the Poisson spot experiment, we show that a tubular cone of x-rays incident upon a crystalline sample produces diffraction spots or foci, corresponding to Bragg maxima within a transmission shadow. We discuss the beam geometry and the intensity gain recorded at the foci in transmission mode. We describe the geometric growth and decay of the foci over a linear axis with the aid of a movie sequence synchronized with the plotting of a diffractogram. The mean signal of a small central area in each successive camera image provides the intensity data for the diffractogram. © 2010 American Institute of Physics. ͓doi:10.1063/1.3514235͔The characterization and measurement of crystallographic structure are of fundamental importance in many branches of science. Angular dispersive x-ray diffraction 1 employed routinely for such analysis dominates this field. However, the coherently scattered or diffracted x-ray signatures are weaker, by orders of magnitude, in comparison with the interrogating x-ray beam. State of the art commercially available powder diffractometers may employ highly sensitive large-area detectors with high quantum efficiency and low noise operating over relatively long integration periods.
2This conventional approach is not ideal for the development of scanning techniques and direct imaging applications, which would benefit from higher intensity signals, reduced integration periods, and converging diffracted beams. In this paper we report examples of diffraction image sequences, which demonstrate the growth and collapse of x-ray foci along the symmetry axis of a tubular interrogating x-ray beam.3 Our approach embodies an analog, employing x-rays, of the optical phenomenon that produces an intensity maximum, known as Poisson's spot, 4 at the center of the geometric shadow of circular opaque objects. In common with short wavelength Poisson spot techniques employing x-ray zone plates 5 or molecular beams 6 we measure the relative intensity of diffraction maxima at the center of a circular geometric shadow. Unlike these techniques, we employ an annular zone, defined at the intersection of a tubular cone of x-rays and a crystalline sample, enabling constructive on-axis interference to form intense spots or foci. The relative intensity and distribution of the foci correspond to the Bragg maxima determined by the crystalline structure of the sample.Consideration of diffraction patterns composed of individual Debye ring contributions hypothesizes the formation of a Poisson spot analog in Fig. 1. A tubular cone of x-rays with its symmetry axis incident normally upon a planar polycrystalline sample and image plane Í‘positioned on the transmission side of the sampleÍ’ will produce a continuum of relatively inclined Debye cones resulting in planar patterns composed of elliptical rings. The resultant circular termini and spot intensity fluctuations are due to rotatio...