Fe3O4@TiO2 nanoparticles catalyzed and NaBH4 assisted one-pot reductive amination of aldehydes at ambient condition

Pinjari, Sajid; Shirole, Gopinath; Uphade, Bhagwat; Gadhave, Anil

doi:10.1007/s11164-023-05123-2

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2024

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“…Therefore there is still a need to develop a more efficient environmentally benign methods for the synthesis of 1,8-dioxodecahydroacridine derivatives. With this view and in continuation to our work in the development of new methods for synthesis of important heterocyclic compounds, [34][35][36] herein we report aluminized polyborate as mild solid acid catalyst for the green and efficient synthesis of 1,8-dioxo-decahydroacridines with good product yield under solvent free conditions.…”

Section: Introductionmentioning

confidence: 72%

Aluminized polyborate catalyzed efficient solvent-free synthesis of 1,8-dioxo-decahydroacridines via hantzsch condensation

Aute,

Parhad,

Vikhe

et al. 2024

10.5267/j.ccl

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In this work we report, aluminized polyborate catalyzed facile and efficient one-pot four component Hantzsch synthesis of 1,8-dioxo-decahydroacridines using substituted aromatic aldehydes (1 mmol), dimedone (2 mmol) and ammonium acetate (1.5 mmol) at 95-100oC under solvent-free condition. The prominent advantages of this methodology are good product yields (85-95%), eco-friendliness, mild reaction conditions and use of inexpensive catalyst. The structures of the targeted molecules were examined by FT-IR, 1H-NMR and mass spectral techniques.

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Section: Introductionmentioning

confidence: 72%