2015
DOI: 10.1016/j.talanta.2015.06.046
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Fast vaporization solid phase microextraction and ion mobility spectrometry: A new approach for determination of creatinine in biological fluids

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Cited by 15 publications
(5 citation statements)
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“…When GFR is less than 15 mL/min per 1.73 m 2 , it is a sign and symptom of uremia, which requires dialysis or kidney transplantation . A variety of methods, therefore, have been developed for quantitative detection of creatinine, such as capillary electrophoresis, gas chromatography, liquid chromatography, mass spectrometry, and so on besides the mostly used strategy of Jaffe’s method and enzymatic digestion in clinical trials. Actually, the colorimetric method, such as Jaffe’s method, is one of simplest, most convenient, and promising methods with not only fast naked eye-distinguishable results but quantitative determination by UV–vis spectrometer. However, picric acid forms an orange complex not only with creatinine but also with many other biomolecules (e.g., metabolins and drugs) in alkaline media.…”
Section: Introductionmentioning
confidence: 99%
“…When GFR is less than 15 mL/min per 1.73 m 2 , it is a sign and symptom of uremia, which requires dialysis or kidney transplantation . A variety of methods, therefore, have been developed for quantitative detection of creatinine, such as capillary electrophoresis, gas chromatography, liquid chromatography, mass spectrometry, and so on besides the mostly used strategy of Jaffe’s method and enzymatic digestion in clinical trials. Actually, the colorimetric method, such as Jaffe’s method, is one of simplest, most convenient, and promising methods with not only fast naked eye-distinguishable results but quantitative determination by UV–vis spectrometer. However, picric acid forms an orange complex not only with creatinine but also with many other biomolecules (e.g., metabolins and drugs) in alkaline media.…”
Section: Introductionmentioning
confidence: 99%
“…Solid phase microextraction (SPME) coupled to ultrafast evaporation with ion mobility spectrometry (IMS) readout has been proposed by Jafari et al (2015). The approach was validated with the Jaffé method in two serum and urine samples showing recovery values close to 100%.…”
Section: Other Methodsmentioning
confidence: 99%
“…A glass bath and a heater/stirrer were used to adjust the rotation speed and the extraction temperature. A home‐made thermoelectric cooler was employed to cool the fibers during extraction. The solutions were under the corresponding extraction conditions for 2 min to reach equilibrium, before starting each extraction procedure.…”
Section: Methodsmentioning
confidence: 99%
“…A single SPME fiber may be used several times. In the two last decades many homemade SPME fibers have been used in numerous media including environmental and biological media. Other aspects of the SPME methods have been reviewed elsewhere .…”
Section: Introductionmentioning
confidence: 99%