Fabrication of «TiC-HSS Steel Binder» Composite Powders by Self-Propagating High Temperature Synthesis

Коростелева, Е. Н.; Прибытков, Г. А.; Krinitcyn, M. G.; Baranovskii, A. V.; Коржова, В. В.; Strel’nitskij, V.E.

doi:10.4028/www.scientific.net/kem.712.195

Cited by 6 publications

(3 citation statements)

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“…It was found that the non-equilibrium metal-matrix structure of the powders formed as a result of SHS by the layerwise combustion method consisting mainly of non-stoichiometric titanium carbide [30,31]. Many works are devoted to the non-stoichiometricity of titanium carbide [6,[8][9][10].…”

Section: Resultsmentioning

confidence: 99%

“…The combustion product remains of titanium silicide were removed after synthesis; the reacted compact was milled and sieved into fractions. Using this procedure, synthesized powders of all investigated compositions containing titanium carbide were obtained [28][29][30][31][32]. The typical microstructure and morphology of the studied synthesized powder compositions are shown in Figure 1.…”

Section: Materials and Experimental Proceduresmentioning

confidence: 99%

“…In the second case, the excess carbon content is desirable in order to achieve an acceptable volume fraction of carbide. The method of producing a metal matrix composite by the SHS method is quite simple when the synthesis takes place directly during the reaction of titanium and carbon in the presence of a thermally-inert metal matrix [28][29][30]. In this case, a structure with carbides surrounded by a metal binder is formed directly during the synthesis process.…”

Section: Introductionmentioning

confidence: 99%

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Sintering Behavior and Microstructure of TiC-Me Composite Powder Prepared by SHS

Коростелева

Коржова

Krinitcyn

2017

Metals

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Titanium, its alloys, and refractory compounds are often used in the compositions of surfacing materials. In particular, under the conditions of electron-beam surfacing the use of synthesized composite powder based on titanium carbide with a metal binder (TiC-Me) has a positive effect. These powders have been prepared via the self-propagating high-temperature synthesis (SHS) present in a thermally-inert metal binder. The initial carbide particle distribution changes slightly in the surfacing layer in the high-energy rapid process of electron-beam surfacing. However, these methods also have their limitations. The development of technologies and equipment using low-energy sources is assumed. In this case, the question of the structure formation of composite materials based on titanium carbide remains open, if a low-energy and prolonged impact in additive manufacturing will be used. This work reports the investigation of the sintered powders that were previously synthesized by the layerwise combustion mode of a mixture of titanium, carbon black, and metal binders of various types. The problems of structure formation during vacuum sintering of multi-component powder materials obtained as a result of SHS are considered. The microstructure and dependences of the sintered composites densification on the sintering temperature and the composition of the SH-synthesized powder used are presented. It has been shown that under the conditions of the nonstoichiometric synthesized titanium carbide during subsequently vacuum sintering an additional alloy formation occurs that can lead to a consolidation (shrinkage) or volumetric growth of sintered TiC-Me composite depending on the type of metal matrix used.

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