Abstract:We show with multiple luminescence dating techniques that the sedimentary record for Lake Eyre, Australia's largest lake, extends beyond 200 thousand years (ka) to Marine Isotope Stage (MIS) 7. Transgressive clayey sand and finely laminated clays overlying the Miocene Etadunna Formation in Lake Eyre North document the deep-lake phases of central South Australia in the past. Until now, unresolved chronology has hampered our ability to interpret these sedimentary records, which are important for understanding th… Show more
“…Multigrain residual D e values of 5-19 Gy have been reported for several modern aeolian sediments from Eurasia and South Africa (see Duller and Wintle, 2012). Arnold et al (2014) reported a similarly sized multigrain D e of 7.3 ± 0.8 Gy for a modern slopewash and aeolian deposit from north-central Spain, while multi-grain residual D e values of several tens of Gy have been obtained for coastal and lacustrine shoreline deposits from South Africa and Australia (Jacobs et al, 2011;Fu et al, 2017). In contrast, very large multi-grain TT-OSL residual doses of 250-300 Gy have been reported for modern suspended sediments and overbank deposits from the Yellow River (Hu et al, 2010), potentially cautioning against the suitability of TT-OSL dating in turbid and UVdepleted fluvial settings.…”
Section: Introductionmentioning
confidence: 88%
“…Thirteen samples were collected from actively accumulating, or very recently accumulated, surface sediment deposits that were expected to yield burial doses close to, or consistent with, 0 Gy (assuming adequate signal bleaching during transportation). These samples represent modern analogues for associated archaeological, palaeontological and palaeoenvironmental dating samples being studied as part of recent or ongoing TT-OSL dating projects (e.g., Arnold et al, 2014;Demuro et al, 2014;Fu et al, 2017). Two shallow cave infill samples from the middle Pleistocene palaeoanthropological sites of Galería and Sima del Elefante, Atapuerca, (ATG10-3, ATE10-13) have been chosen for the daylight bleaching experiments, owing to their relatively high and comparable mean burial doses, and uniformly bleached single-grain TT-OSL D e distributions (e.g., Demuro et al, 2014;.…”
Section: Sample Details and Experimental Proceduresmentioning
confidence: 99%
“…While these various TT-OSL bleaching assessments have proved insightful, they are based on a relatively modest number of observations (n = < 20 samples) and further work is needed to better characterise TT-OSL signal resetting across a broader range of natural contexts using complementary types of experimental procedures. Additionally, all existing assessments of TT-OSL bleaching characteristics, with the exception of one study (Fu et al, 2017), have been performed at the multi-grain scale of D e analysis. It remains unclear, therefore, whether TT-OSL residual doses reported in existing modern analogue studies partly reflect averaging effects arising from simultaneously measuring grains with different bleaching histories, signal compositions or TT-OSL source trap properties.…”
Section: Introductionmentioning
confidence: 99%
“…Single-grain TT-OSL has recently been applied at several independently dated archaeological sites from Spain and Australia (e.g., Demuro et al, 2014;Hamm et al, 2016). These single-grain studies have also revealed that multi-grain TT-OSL signals may be dominated by grains with unfavourable TT-OSL behaviours (e.g., and that apparent multi-grain TT-OSL residual doses of several tens of Gy may result from the inclusion of grain types that are routinely rejected by single-grain quality assurance criteria (Fu et al, 2017). Such complications require further examination, and additional single-grain bleaching assessments are needed to better characterise TT-OSL signal resetting at the most fundamental scale of D e analysis.…”
Previous assessments of thermally transferred optically stimulated luminescence (TT-OSL) signal resetting in natural sedimentary settings have been based on relatively limited numbers of observations, and have been conducted primarily at the multi-grain scale of equivalent dose (D e) analysis. In this study, we undertake a series of single-grain TT-OSL bleaching assessments on nineteen modern and geological dating samples from different sedimentary environments. Daylight bleaching experiments performed over several weeks confirm that singlegrain TT-OSL signals are optically reset at relatively slow, and potentially variable, rates. Single-grain TT-OSL residual doses range between 0 and 24 Gy for thirteen modern samples, with > 50% of these samples yielding weighted mean D e values of 0 Gy at 2σ. Single-grain OSL and TT-OSL dating comparisons performed on wellbleached and heterogeneously bleached late Pleistocene samples from Kangaroo Island, South Australia, yield consistent replicate age estimates. Our results reveal that (i) single-grain TT-OSL residuals can potentially be reduced down to insignificant levels when compared with the natural dose range of interest for most TT-OSL dating applications; (ii) the slow bleaching properties of TT-OSL signals may not necessarily limit their dating applicability to certain depositional environments; and (iii) non-trivial differences may be observed between single-grain and multi-grain TT-OSL bleaching residuals in some modern samples. Collectively, these findings suggest that single-grain TT-OSL dating may offer advantages over multi-grain TT-OSL dating in certain complex depositional environments.
“…Multigrain residual D e values of 5-19 Gy have been reported for several modern aeolian sediments from Eurasia and South Africa (see Duller and Wintle, 2012). Arnold et al (2014) reported a similarly sized multigrain D e of 7.3 ± 0.8 Gy for a modern slopewash and aeolian deposit from north-central Spain, while multi-grain residual D e values of several tens of Gy have been obtained for coastal and lacustrine shoreline deposits from South Africa and Australia (Jacobs et al, 2011;Fu et al, 2017). In contrast, very large multi-grain TT-OSL residual doses of 250-300 Gy have been reported for modern suspended sediments and overbank deposits from the Yellow River (Hu et al, 2010), potentially cautioning against the suitability of TT-OSL dating in turbid and UVdepleted fluvial settings.…”
Section: Introductionmentioning
confidence: 88%
“…Thirteen samples were collected from actively accumulating, or very recently accumulated, surface sediment deposits that were expected to yield burial doses close to, or consistent with, 0 Gy (assuming adequate signal bleaching during transportation). These samples represent modern analogues for associated archaeological, palaeontological and palaeoenvironmental dating samples being studied as part of recent or ongoing TT-OSL dating projects (e.g., Arnold et al, 2014;Demuro et al, 2014;Fu et al, 2017). Two shallow cave infill samples from the middle Pleistocene palaeoanthropological sites of Galería and Sima del Elefante, Atapuerca, (ATG10-3, ATE10-13) have been chosen for the daylight bleaching experiments, owing to their relatively high and comparable mean burial doses, and uniformly bleached single-grain TT-OSL D e distributions (e.g., Demuro et al, 2014;.…”
Section: Sample Details and Experimental Proceduresmentioning
confidence: 99%
“…While these various TT-OSL bleaching assessments have proved insightful, they are based on a relatively modest number of observations (n = < 20 samples) and further work is needed to better characterise TT-OSL signal resetting across a broader range of natural contexts using complementary types of experimental procedures. Additionally, all existing assessments of TT-OSL bleaching characteristics, with the exception of one study (Fu et al, 2017), have been performed at the multi-grain scale of D e analysis. It remains unclear, therefore, whether TT-OSL residual doses reported in existing modern analogue studies partly reflect averaging effects arising from simultaneously measuring grains with different bleaching histories, signal compositions or TT-OSL source trap properties.…”
Section: Introductionmentioning
confidence: 99%
“…Single-grain TT-OSL has recently been applied at several independently dated archaeological sites from Spain and Australia (e.g., Demuro et al, 2014;Hamm et al, 2016). These single-grain studies have also revealed that multi-grain TT-OSL signals may be dominated by grains with unfavourable TT-OSL behaviours (e.g., and that apparent multi-grain TT-OSL residual doses of several tens of Gy may result from the inclusion of grain types that are routinely rejected by single-grain quality assurance criteria (Fu et al, 2017). Such complications require further examination, and additional single-grain bleaching assessments are needed to better characterise TT-OSL signal resetting at the most fundamental scale of D e analysis.…”
Previous assessments of thermally transferred optically stimulated luminescence (TT-OSL) signal resetting in natural sedimentary settings have been based on relatively limited numbers of observations, and have been conducted primarily at the multi-grain scale of equivalent dose (D e) analysis. In this study, we undertake a series of single-grain TT-OSL bleaching assessments on nineteen modern and geological dating samples from different sedimentary environments. Daylight bleaching experiments performed over several weeks confirm that singlegrain TT-OSL signals are optically reset at relatively slow, and potentially variable, rates. Single-grain TT-OSL residual doses range between 0 and 24 Gy for thirteen modern samples, with > 50% of these samples yielding weighted mean D e values of 0 Gy at 2σ. Single-grain OSL and TT-OSL dating comparisons performed on wellbleached and heterogeneously bleached late Pleistocene samples from Kangaroo Island, South Australia, yield consistent replicate age estimates. Our results reveal that (i) single-grain TT-OSL residuals can potentially be reduced down to insignificant levels when compared with the natural dose range of interest for most TT-OSL dating applications; (ii) the slow bleaching properties of TT-OSL signals may not necessarily limit their dating applicability to certain depositional environments; and (iii) non-trivial differences may be observed between single-grain and multi-grain TT-OSL bleaching residuals in some modern samples. Collectively, these findings suggest that single-grain TT-OSL dating may offer advantages over multi-grain TT-OSL dating in certain complex depositional environments.
“…The abundance of quartz dominated landscapes and the poor preservation of organic remains for other radiometric techniques has resulted in a dominance of the approach in recent literature (e.g. ; Fitzsimmons et al, 2014;Fu et al, 2017;Hughes et al, 2014;Williams et al, 2014Williams et al, , 2017. To date, however, the technique has largely focussed on Indigenous archaeological sites, often of considerable age (Dortch et al, 2016;Veth et al, 2017).…”
While exploration of Australian post-colonial (≤0.25 ka) OSL dating is well established in a range of natural sedimentary contexts (e.g. fluvial, aeolian, coastal), to date there have been no successful examples of the technique applied to archaeological sediments of this era. Here we present the results of a multi-phase compliance-based archaeological excavations of a new bridge crossing the Hawkesbury-Nepean River (northwest Sydney). These works identified a Last Glacial Maximum (LGM) aeolian deposit through which a colonial era drainage system had been excavated. Historical documents reveal the construction of the system occurred between 1814 and 1816 CE. An opportunistic range-finding Optically Stimulated Luminescence (OSL) sample was obtained from anthropogenic trench backfillcomposed of reworked LGM depositsimmediately above the drainage system. Minimum and Finite Mixture age models of single grain quartz OSL provided a date of 1826 CE (1806-1846 CE), in close agreement with the documented age of construction. These findings provide the first evidence of a colonial structure reliably dated using OSL, and demonstrate the feasibility of wider deployment of OSL dating to other archaeological sites of the recent era (≤0.25 ka). We propose that such environments associated with large volumes of sand-rich backfill, in particular, likely heighten OSL dating success. We propose that well-documented historical archaeological sites in Australia also have the potential to provide a robust testing ground for further evaluating the accuracy of OSL dating in a range of young archaeological sedimentary contexts, potentially to sub-decadal levels.
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