To study the influence
of different confining pressures on the
pore structure and connectivity of high-rank coal, the high-rank raw
coal of the Shanxi Xinjing Mine No. 9 coal seam was studied. A low-field
nuclear magnetic resonance (LNMR) test system and a vacuum pressurized
water saturation system were used to analyze the samples. The
T
2
spectra of samples, saturated with water under
different confining pressures and containing residual water after
centrifugation, were tested. The coal sample pore size distributions,
permeabilities, free fluid values, bound fluid values, and other parameters
were obtained, and a calculation model of the coal pore connectivity
ratio was established. The results were as follows. When the saturated
pressures were 5, 10, 15, 20, 25, and 30 MPa, the pore diameters of
the coal samples were mainly concentrated in the ranges of 0.00023–0.069
and 1.29–24.09 μm. Among them, micropores (<10 nm)
and small pores (10 < 100 nm) account for the main part, mesopores
(100 < 1000 nm) were underdeveloped, and relatively few macropores
(>1000 nm) and fissures developed. As the confining pressure increased,
the coal porosity and connectivity showed a trend of decreasing, then
increasing, and finally remaining basically unchanged. The total pore
connectivity rates of the coal samples were 37.0–62.6%. The
interconnection rates of the micropores, small holes, mesopores, and
macropores are 2.90–34.55, 89.09–99.03, 97.09–100,
and 100%, respectively. The total pore connectivity followed an exponential
functional relationship with permeability, and the critical confining
pressure of high-rank coal was 25 MPa. These results provide a scientific
basis for the high-pressure water injection of high-rank coal seams.