This experimental work explores the flow field around a three-dimensional expansion–compression geometry on a slender cone at Mach 8 using high-frequency pressure sensors, high-frame-rate schlieren, temperature-sensitive paint, shear-stress measurements and oil-flow visualizations. The
$7^\circ$
cone geometry has a hyperbolic slice which acts as an expansion corner and suppresses the disturbances present in the upstream boundary layer. Downstream of the cone-slice corner, high-frequency boundary-layer disturbances attenuate in all cases. Under laminar conditions, second-mode instabilities from the cone diminish and lower-frequency second-mode waves develop on the slice at a frequency commensurate with the increased boundary layer thickness. For fully turbulent cases, the boundary layer over the slice shows evidence of a two-layered nature with a turbulent outer region and a near-wall region with strong attenuation of high-frequency disturbances and reappearance of lower-frequency instability waves. When a downstream compression ramp is added to the slice, the expanded boundary layer shows enhanced susceptibility to separation such that separation is observed at a
$10^{\circ }$
deflection, which is smaller than expected for turbulent conditions. For a
$30^{\circ }$
ramp, boundary-layer separation occurs further upstream where the heat flux contours show a decrease in heating that is characteristic of a transitional separation. These results demonstrate the effect of relaminarization caused by an upstream expansion on a subsequent shock-wave/boundary-layer interaction.