2011
DOI: 10.1007/s11665-011-9986-0
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Experimental Determination of the Interparticle Contact Structure in Densified Iron Powders

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“…The disadvantage of the chromato graphic analysis is a long term measurement (up to 8 h per sample). Therefore, a modified probe method was applied [17][18][19][20], which was based on the use of the time dependence of the integral intensity of a mass spec trum with a subsequent processing of kinetic data ("wave form") using a Fourier transformation. The essence of the method is that: a preliminary degasified sample is processed under pressure of a gas having a relatively small molecular weight and inert to the sample material.…”
Section: Experimental and Discussionmentioning
confidence: 99%
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“…The disadvantage of the chromato graphic analysis is a long term measurement (up to 8 h per sample). Therefore, a modified probe method was applied [17][18][19][20], which was based on the use of the time dependence of the integral intensity of a mass spec trum with a subsequent processing of kinetic data ("wave form") using a Fourier transformation. The essence of the method is that: a preliminary degasified sample is processed under pressure of a gas having a relatively small molecular weight and inert to the sample material.…”
Section: Experimental and Discussionmentioning
confidence: 99%
“…It is also clear that the stress-strain state of the polymer on these regions depends on the hole diameter. Earlier it was found that in the absence of mechanical stresses the degassing kinetic curve shape depends on the sample structure and not on its form and sizes [17].…”
Section: Experimental and Discussionmentioning
confidence: 99%