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AcknowledgmentsThe work described in this thesis represents the results of collaborations with many people, all of whom I owe a great debt of gratitude. I have had a unique opportunity as a graduate student to work with some of the best scientists in the field and I have learned and benefited from all of them.First I want to thank Mike Perry. Mike has aided me through my graduate career in too many ways to summarize here. I have learned many things, both in science and otherwise, from Mike. Mike was a very strong supporter of me and my efforts from the earliest days in his group, and I immensely value his support, suggestions and complements. Mike is also to be lauded for supplying me with a world class atmosphere to do physics. He has gone beyond the call of duty in providing me with intellectual as well as physical resources that are unparalleled for most graduate students. In general, the studies of this manuscript fall into three categories. First, a unique 130 fs, 8 TW laser that is based on chirped pulse amplification, is described, and its performance is evaluated. In particular, a detailed analysis of flashlamp pumping large aperture (> 1 cm) LiSAF amplifiers is given. The effects of pulse propagation of laser pulses in chirped pulse amplifier lasers is also carelidly examined and modeled.The generation of x-rays through high order harmonics is then discussed with emphasis on characterizing and optimizing harmonic generation. These studies include V an examination of the wavelength range attainable with harmonics, the spatial profiles of the harmonics, the spectral linewidths of the harmonics, and the energy yields of the harmonics.