This
study focuses on the characterization of porous granular materials
for applications in hydraulics of fixed and fluidized beds. Different
density measurement procedures were tested using five different sieved
fractions of each of zeolite, activated carbon, and anthracite coal
media to compare these procedures and to ascertain the effect of the
density measurement method used on the calculation of other particle
and bed properties. The mentioned particle and bed properties are
the following: (i) particle density, (ii) particle size (equivalent
diameter), (iii) sphericity, (iv) fixed-bed porosity, and (v) expanded-bed
porosity during fluidization. The density of each of the 15 fractions
was determined using four different methods: (i) cone test (ASTM C128-12),
(ii) Le Châtelier flask method, (iii) soaking and straining,
and (iv) skeletal density. The first three of these measure “wet
density” (i.e., pores filled with liquid), the difference between
them being in how the particles are saturated with liquid before the
density determinations. The results show that the standard cone test
is the most suitable method for the type of applications considered
in this work whereas the use of other simpler methods leads to varying
degrees of error. An important finding of this work is that the fluidized-bed
expansion data of the porous media studied here are in excellent agreement
with the predictions of a correlation that Soyer and Akgiray (J. Water Supply: Res. Technol.--AQUA, 2009, 58, 336) developed by testing nonporous materials only.