“…Compound 8 is very soluble in CH,Cl, and thf and moderately soluble in non-polar organic solvents and MeOH. IR: v(C0) (cyclohexane) 2056s, 2 0 2 2 5 2 0 0 6 ~ 1993s, 1986m, 1972(sh), 1962s, 1951m, 1942(sh) [10][11][12][13][14]. Two check reflections showed no decay during the experiment and an empirical y-scan absorption correction based on three reflections was applied (transmission: minimum 86.7, maximum 100.0%) as well as Lorentz and polarisation corrections.…”