Abstract. Surface treatment of three natural fibers including cellulose (CE), sawdust (SD) and wheat straw (WS) were carried out with triethoxysilane (AS), methacriloxy propyl trimethoxy silane (MS), and maleic anhydride grafted polypropylene (MAPP), respectively. Then the composites reinforced by these natural fibers were studied by water absorption and FTIR. It was found that water absorption decreased with employment of coupling agents. Among the coupling agents, MAPP exhibited the best performance in decreasing water absorption. In addition, FTIR analysis revealed the decrease in hydrophilicity of fibers with silane treatment and new bond formations with employment of MAPP.