Abstract:Cyclic voltammetry of a DMSO2–AlCl3 electrolyte was performed using an ultramicro disk electrode to evaluate the effects of ammonium salts on the Al electrodeposition reaction. A side reaction in the electrolyte at potentials more negative than −0.8 V (versus Al-wire) was found to suppress the Al electrodeposition reaction. The addition of even a small amount of NH4Cl promoted an Al electrodeposition reaction, which proceeded at more positive potentials than the side reaction. With the excessive addition of te… Show more
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