“…2H, s),5.88 (1H, s), 7.14-7.16 (2H, m), 7.23-7.32 (3H, m) ppm;13 C NMR (75.5 MHz, CDCl 3 ): δ 21.1, 48.7, 56.7, 72.1, 95.3, 126.7, 127.5, 128.8, 136.3, 147.9, 162.2, 166.7 ppm; HRMS (ESI) m/z calcd for C 14 H 15 O 2 NI [(M + H) + ]: 356.0148, found 356.0141.1-(4-Fluorophenyl)-3-iodo-4-methoxy-6-methylpyridin-2(1H)-one, 30 2 equiv. N-iodosuccinimide required.…”