Abstract:In this work, a new analytical approach based on proton nuclear magnetic resonance spectroscopy has been optimized for the direct estimation of different phenolic components in a phosphate ester sample. In high resonance proton nuclear magnetic resonance spectrum of fire resistance hydraulic fluids, methyl protons of cresyl, xylyl, and other phosphates (ethyl, propyl, and butyl) are unambiguously distinguished by their different chemical shift and used for quantitative estimation. The developed methodology was… Show more
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