“…20 The disappearance of the (001) peak and the emergence of a new diffraction peak at 2y = 241 in the XRD pattern of rGO demonstrates that graphite oxide has been well reduced. 20 The NiCo-LDH sample exhibits five characteristic diffraction peaks at 2y values of 11.11, 22.11, 34.41, 38.61, and 60.71, which can be indexed to the (003), ( 006), (009), ( 015) and (110) planes of hydrotalcite-like LDH phase in good agreement with previous reports. 21,22 The XRD pattern of the NiCo-LDH@rGO catalyst retains the corresponding peaks of pure NiCo-LDH, revealing the existence of NiCo-LDH in the composite without affecting the crystalline phase of LDH.…”